(6-Hydroxyhex-1-en-1-yl)boronic acid

Base Information Edit

Chemical Name:(6-Hydroxyhex-1-en-1-yl)boronic acid
CAS No.:132047-94-0
Molecular Formula:C6H13BO3
Molecular Weight:143.98
Hs Code.:
DSSTox Substance ID:DTXSID00697717
Mol file:132047-94-0.mol

Synonyms:DTXSID00697717;(6-Hydroxyhex-1-en-1-yl)boronic acid

Suppliers and Price of (6-Hydroxyhex-1-en-1-yl)boronic acid

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 4 raw suppliers

Chemical Property of (6-Hydroxyhex-1-en-1-yl)boronic acid Edit

Chemical Property:

PSA：60.69000
LogP:-0.28280
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:144.0957744
Heavy Atom Count:10
Complexity:93

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B(C=CCCCCO)(O)O

Technology Process of (6-Hydroxyhex-1-en-1-yl)boronic acid

There total 2 articles about (6-Hydroxyhex-1-en-1-yl)boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 928-90-5
5-hexyl-1-ol

: 55671-55-1,146732-64-1
dibromoborane-methyl sulfide complex

: 132047-94-0
(E)-6-hydroxyhex-1-en-ylboronic acid

Guidance literature:: In dichloromethane; B-compd. soln. addn. slowly to org. compd. soln. at 0°C, soln. allowing to warm to room temp., stirring 30 min, refluxing overnight (50°C), pouring into H2O/Et2O 1:1 at 0°C, stirring 2 h, aq. layer sepn., extn. (Et2O), combined org.; layer and extracts drying (MgSO4), evapn. (reduced pressure), solid recrystn. (toluene);
DOI:10.1039/P19950002083