Benzenepropanamide, N-(6-amino-1,2,3,4-tetrahydro-3-methyl-2,4-dioxo-1-propyl-5-pyrimidinyl)-

Base Information

Chemical Name:Benzenepropanamide, N-(6-amino-1,2,3,4-tetrahydro-3-methyl-2,4-dioxo-1-propyl-5-pyrimidinyl)-
CAS No.:132940-70-6
Molecular Formula:C17H22N4O3
Molecular Weight:330.38
Hs Code.:
Mol file:132940-70-6.mol

Synonyms:Benzenepropanamide, N-(6-amino-1,2,3,4-tetrahydro-3-methyl-2,4-dioxo-1-propyl-5-pyrimidinyl)-

Suppliers and Price of Benzenepropanamide, N-(6-amino-1,2,3,4-tetrahydro-3-methyl-2,4-dioxo-1-propyl-5-pyrimidinyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of Benzenepropanamide, N-(6-amino-1,2,3,4-tetrahydro-3-methyl-2,4-dioxo-1-propyl-5-pyrimidinyl)-

Chemical Property:

PSA：102.61000
LogP:2.34120

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenepropanamide, N-(6-amino-1,2,3,4-tetrahydro-3-methyl-2,4-dioxo-1-propyl-5-pyrimidinyl)-

There total 3 articles about Benzenepropanamide, N-(6-amino-1,2,3,4-tetrahydro-3-methyl-2,4-dioxo-1-propyl-5-pyrimidinyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53681-48-4
6-amino-3-methyl-1-propyl-1H-pyrimidine-2,4-dione

: 132940-70-6
N-(6-Amino-3-methyl-2,4-dioxo-1-propyl-1,2,3,4-tetrahydro-pyrimidin-5-yl)-3-phenyl-propionamide

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / NaNO₂, AcOH / H₂O / 90 °C

2: 67 percent / H₂ / 5percent Pd/C / ethanol / 24 h / 3102.9 Torr

3: CH₂Cl₂ / 1.) 5 deg C, 15 min, 2.) RT, 30 min

With hydrogen; acetic acid; sodium nitrite; palladium on activated charcoal; In ethanol; dichloromethane; water;
DOI:10.1021/jm00108a029

Reference yield:

: 116545-96-1
6-amino-3-methyl-5-nitroso-1-n-propyluracil

: 132940-70-6
N-(6-Amino-3-methyl-2,4-dioxo-1-propyl-1,2,3,4-tetrahydro-pyrimidin-5-yl)-3-phenyl-propionamide

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / H₂ / 5percent Pd/C / ethanol / 24 h / 3102.9 Torr

2: CH₂Cl₂ / 1.) 5 deg C, 15 min, 2.) RT, 30 min

With hydrogen; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jm00108a029