Cyclohexanecarboxamide, N-(6-amino-1,2,3,4-tetrahydro-3-methyl-2,4-dioxo-1-propyl-5-pyrimidinyl)-

Base Information

Chemical Name:Cyclohexanecarboxamide, N-(6-amino-1,2,3,4-tetrahydro-3-methyl-2,4-dioxo-1-propyl-5-pyrimidinyl)-
CAS No.:132940-67-1
Molecular Formula:C15H24N4O3
Molecular Weight:308.38
Hs Code.:
Mol file:132940-67-1.mol

Synonyms:Cyclohexanecarboxamide, N-(6-amino-1,2,3,4-tetrahydro-3-methyl-2,4-dioxo-1-propyl-5-pyrimidinyl)-

Suppliers and Price of Cyclohexanecarboxamide, N-(6-amino-1,2,3,4-tetrahydro-3-methyl-2,4-dioxo-1-propyl-5-pyrimidinyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of Cyclohexanecarboxamide, N-(6-amino-1,2,3,4-tetrahydro-3-methyl-2,4-dioxo-1-propyl-5-pyrimidinyl)-

Chemical Property:

PSA：99.12000
LogP:1.71220

Purity/Quality:: 99% ，98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclohexanecarboxamide, N-(6-amino-1,2,3,4-tetrahydro-3-methyl-2,4-dioxo-1-propyl-5-pyrimidinyl)-

There total 3 articles about Cyclohexanecarboxamide, N-(6-amino-1,2,3,4-tetrahydro-3-methyl-2,4-dioxo-1-propyl-5-pyrimidinyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53681-48-4
6-amino-3-methyl-1-propyl-1H-pyrimidine-2,4-dione

: 132940-67-1
Cyclohexanecarboxylic acid (6-amino-3-methyl-2,4-dioxo-1-propyl-1,2,3,4-tetrahydro-pyrimidin-5-yl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / NaNO₂, AcOH / H₂O / 90 °C

2: 67 percent / H₂ / 5percent Pd/C / ethanol / 24 h / 3102.9 Torr

3: pyridine / CH₂Cl₂ / 1.) 5 deg C, 15 min, 2.) RT, 30 min

With pyridine; hydrogen; acetic acid; sodium nitrite; palladium on activated charcoal; In ethanol; dichloromethane; water;
DOI:10.1021/jm00108a029

Reference yield:

: 116545-96-1
6-amino-3-methyl-5-nitroso-1-n-propyluracil

: 132940-67-1
Cyclohexanecarboxylic acid (6-amino-3-methyl-2,4-dioxo-1-propyl-1,2,3,4-tetrahydro-pyrimidin-5-yl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / H₂ / 5percent Pd/C / ethanol / 24 h / 3102.9 Torr

2: pyridine / CH₂Cl₂ / 1.) 5 deg C, 15 min, 2.) RT, 30 min

With pyridine; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jm00108a029