Cyclobutanecarboxaldehyde, 2-(1-methoxyethyl)-, [1S-[1alpha,2alpha(R*)]]- (9CI)

Base Information

Chemical Name:Cyclobutanecarboxaldehyde, 2-(1-methoxyethyl)-, [1S-[1alpha,2alpha(R*)]]- (9CI)
CAS No.:133796-83-5
Molecular Formula:C8H14O2
Molecular Weight:142.19556
Hs Code.:
Mol file:133796-83-5.mol

Synonyms:Cyclobutanecarboxaldehyde, 2-(1-methoxyethyl)-, [1S-[1alpha,2alpha(R*)]]- (9CI)

Suppliers and Price of Cyclobutanecarboxaldehyde, 2-(1-methoxyethyl)-, [1S-[1alpha,2alpha(R*)]]- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Cyclobutanecarboxaldehyde, 2-(1-methoxyethyl)-, [1S-[1alpha,2alpha(R*)]]- (9CI)

Chemical Property:

PSA：26.30000
LogP:1.24640

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclobutanecarboxaldehyde, 2-(1-methoxyethyl)-, [1S-[1alpha,2alpha(R*)]]- (9CI)

There total 9 articles about Cyclobutanecarboxaldehyde, 2-(1-methoxyethyl)-, [1S-[1alpha,2alpha(R*)]]- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 125109-47-9,125224-60-4,133815-35-7,133815-36-8,133868-06-1,133868-12-9,133868-33-4
(1RS,2RS,1'SR)-1-(1-methoxyethyl)-2-vinylcyclobutane

: 3,5-Bis-[(1R,2S)-2-((R)-1-methoxy-ethyl)-cyclobutyl]-[1,2,4]trioxolane

: 133796-83-5,133868-13-0,133868-22-1,133868-23-2,133868-31-2
(1SR,2RS,1'SR)-2-(1-methoxyethyl)cyclobutanecarboxaldehyde

Guidance literature:: With ozone; In dichloromethane; at -78 ℃;
DOI:10.1021/ja00012a033

Reference yield:

: 125109-46-8,125224-59-1,133868-19-6,133868-20-9,133868-34-5
(1SR,1'RS,2'RS)-1-(2-vinylcyclobutyl)ethanol

: 133796-83-5,133868-13-0,133868-22-1,133868-23-2,133868-31-2
(1SR,2RS,1'SR)-2-(1-methoxyethyl)cyclobutanecarboxaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 82.3 percent / NaH / tetrahydrofuran / 2.5 h / Ambient temperature

2: O₃ / CH₂Cl₂ / -78 °C

With sodium hydride; ozone; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00012a033

Reference yield:

: 125137-90-8
4-Methyl-3-oxa-bicyclo[3.2.0]heptan-2-ol

: 133796-83-5,133868-13-0,133868-22-1,133868-23-2,133868-31-2
(1SR,2RS,1'SR)-2-(1-methoxyethyl)cyclobutanecarboxaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 37.1 percent / tetrahydrofuran / 4.5 h / Ambient temperature

2: 82.3 percent / NaH / tetrahydrofuran / 2.5 h / Ambient temperature

3: O₃ / CH₂Cl₂ / -78 °C

With sodium hydride; ozone; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00012a033