ADIPIC-1,6-13C2 ACID

Base Information

• Chemical Name: ADIPIC-1,6-13C2 ACID
• CAS No.: 133954-44-6
• Molecular Formula: C6H10O4
• Molecular Weight: 148.16
• Mol file: 133954-44-6.mol

Synonyms:ADIPIC-1,6-13C2 ACID;ADIPIC-1,6-13C2 ACID, 99 ATOM % 13C;adipic acid-1,6-13c2;hexanedioc acid-13c2

Chemical Property of ADIPIC-1,6-13C2 ACID

Chemical Property:

• Melting Point: 151-154 °C(lit.)
• Boiling Point: 265 °C100 mm Hg(lit.)
• Flash Point: 385 °F
• PSA: 74.60000
• LogP: 0.71600

Purity/Quality:

98%,99%, ^*data from raw suppliers

AdipicAcid-1,6-13C2 ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 20/22-36
• Safety Statements: 26-36-37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ADIPIC-1,6-13C2 ACID

There total 1 articles about ADIPIC-1,6-13C2 ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

<1,6-(13)C2>-adiponitrile (109432-72-6) → <1,6-(13)C2>adipic acid (133954-44-6)

Guidance literature:

With hydrogenchloride; water; Yield given. Multistep reaction; 1) 50 deg C, 1 h, 2) reflux, 3 h;

DOI:10.1021/ac00053a009

Reference yield:

<1,6-(13)C2>adipic acid (133954-44-6) → cyclopentanone-(13)CO (68488-80-2)

Guidance literature:

potassium fluoride; at 280 - 310 ℃; for 3h; Yield given;

DOI:10.1021/ac00053a009

upstream raw materials:

<1,6-(13)C2>-adiponitrile

Downstream raw materials:

cyclopentanone-⁽¹³⁾CO

Refernces

• 1、 Hall, Randal A.,Jurkiewicz, Antoni,Maciel, Gary E.. "A bicyclic ketone as a solid-state 13C NMR intensity reference". . p. 534 - 538. Retrieved 2007/10/02.