6,7,8,9-TETRAHYDRO-PYRIDO[1,2,A]INDOLE-7-CARBOXYLIC ACID ETHYL ESTER

Base Information

Chemical Name:6,7,8,9-TETRAHYDRO-PYRIDO[1,2,A]INDOLE-7-CARBOXYLIC ACID ETHYL ESTER
CAS No.:135440-73-2
Molecular Formula:C15H17NO2
Molecular Weight:243.3
Hs Code.:
Mol file:135440-73-2.mol

Synonyms:6,7,8,9-TETRAHYDRO-PYRIDO[1,2,A]INDOLE-7-CARBOXYLIC ACID ETHYL ESTER

Suppliers and Price of 6,7,8,9-TETRAHYDRO-PYRIDO[1,2,A]INDOLE-7-CARBOXYLIC ACID ETHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
6,7,8,9-TETRAHYDRO PYRIDO-[1,2,A]INDOLE-7-CARBOXYLIC ACID ETHYL ESTER 95.00%
5MG
$ 503.97

Total 3 raw suppliers

Chemical Property of 6,7,8,9-TETRAHYDRO-PYRIDO[1,2,A]INDOLE-7-CARBOXYLIC ACID ETHYL ESTER

Chemical Property:

PSA：31.23000
LogP:2.76680

Purity/Quality:

97% ^*data from raw suppliers

6,7,8,9-TETRAHYDRO PYRIDO-[1,2,A]INDOLE-7-CARBOXYLIC ACID ETHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6,7,8,9-TETRAHYDRO-PYRIDO[1,2,A]INDOLE-7-CARBOXYLIC ACID ETHYL ESTER

There total 3 articles about 6,7,8,9-TETRAHYDRO-PYRIDO[1,2,A]INDOLE-7-CARBOXYLIC ACID ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 135440-72-1
ethyl 6,7,8,9-tetrahydro-9-oxopyrido<1,2-a>indole-7-carboxylate

: 135440-73-2
ethyl 6,7,8,9-tetrahydropyrido<1,2-a>indole-7 carboxylate

Guidance literature:: With W-2 Raney nickel; In ethanol; water; for 1h; Heating;
DOI:10.1016/S0040-4020(01)86471-1

Reference yield:

: 135440-70-9
diethyl 6,7-dihydro-9-hydroxypyrido<1,2-a>indole-7,8-dicarboxylate

: 135440-73-2
ethyl 6,7,8,9-tetrahydropyrido<1,2-a>indole-7 carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / boric acid / 1.25 h / 150 °C

2: 70 percent / W-2 Raney nickel / ethanol; H₂O / 1 h / Heating

With W-2 Raney nickel; boric acid; In ethanol; water;
DOI:10.1016/S0040-4020(01)86471-1

Reference yield:

: 135440-69-6
ethyl 2-(ethoxycarbonyl)-2,3-dihydro-1-oxo-1H-pyrrolo<1,2-a>indole-2-acetate

: 135440-73-2
ethyl 6,7,8,9-tetrahydropyrido<1,2-a>indole-7 carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / t-BuOK / tetrahydrofuran / 0.25 h / -78 °C

2: 64 percent / boric acid / 1.25 h / 150 °C

3: 70 percent / W-2 Raney nickel / ethanol; H₂O / 1 h / Heating

With W-2 Raney nickel; potassium tert-butylate; boric acid; In tetrahydrofuran; ethanol; water;
DOI:10.1016/S0040-4020(01)86471-1