2-Ethynyl-2,3-dihydro-1H-inden-2-ol

Base Information

Chemical Name:2-Ethynyl-2,3-dihydro-1H-inden-2-ol
CAS No.:136121-30-7
Molecular Formula:C11H10O
Molecular Weight:158.2
Hs Code.:
DSSTox Substance ID:DTXSID20576979
Nikkaji Number:J405.500D
Wikidata:Q82466875
Mol file:136121-30-7.mol

Synonyms:2-Ethynyl-2,3-dihydro-1H-inden-2-ol;136121-30-7;2-ethynyl-1,3-dihydroinden-2-ol;2-ETHYNYL-INDAN-2-OL;2-Ethynylindan-2-ol;DTXSID20576979;MFCD10574829;AKOS006305744;CS-0266199;EN300-1250299;F8883-8267

Suppliers and Price of 2-Ethynyl-2,3-dihydro-1H-inden-2-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-Ethynyl-2,3-dihydro-1H-inden-2-ol

Chemical Property:

Refractive Index:1.611
PSA：20.23000
LogP:1.14950
XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:158.073164938
Heavy Atom Count:12
Complexity:208

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C#CC1(CC2=CC=CC=C2C1)O

Technology Process of 2-Ethynyl-2,3-dihydro-1H-inden-2-ol

There total 3 articles about 2-Ethynyl-2,3-dihydro-1H-inden-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 134970-45-9
2-(1-chloroethenyl)-2-indanol

: 136121-30-7
2-ethynylindene-2-ol

Guidance literature:: With n-butyllithium; In tetrahydrofuran; for 0.7h; -50 up to -40 deg C;
DOI:10.1246/bcsj.64.2153

Reference yield:

: 134970-40-4
2-<1-chloro-1-(p-tolylsulfinyl)ethyl>-2-indanol

: 136121-30-7
2-ethynylindene-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: Heating

2: 92 percent / n-BuLi / tetrahydrofuran / 0.7 h / -50 up to -40 deg C

With n-butyllithium; In tetrahydrofuran;
DOI:10.1246/bcsj.64.2153

Reference yield:

: 615-13-4
2-indanone

: 136121-30-7
2-ethynylindene-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LDA / 1.) THF

2: Heating

3: 92 percent / n-BuLi / tetrahydrofuran / 0.7 h / -50 up to -40 deg C

With n-butyllithium; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1246/bcsj.64.2153