Technology Process of 5,7-Octadecadiynoic acid
There total 6 articles about 5,7-Octadecadiynoic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dipyridinium dichromate;
In
N,N-dimethyl-formamide;
Ambient temperature;
DOI:10.1021/jo00025a045
- Guidance literature:
-
With
pyrrolidine; copper(l) iodide;
at 20 ℃;
for 3h;
DOI:10.1021/ma101264k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1) n-butyllithium / 1) THF, -23 deg C, 1 h, 2) THF, HMPA, 2.1) -23 deg C, 30 min., 2.2) RT, 1.5 h
2: 93 percent / 37percent HCl / methanol / Ambient temperature
3: 60 percent / pyridinium dichromate / dimethylformamide / Ambient temperature
With
hydrogenchloride; dipyridinium dichromate; n-butyllithium;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00025a045
