Technology Process of Oxiranemethanol, 3-(3-methyl-3-butenyl)- (9CI)
There total 1 articles about Oxiranemethanol, 3-(3-methyl-3-butenyl)- (9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
aluminium hydride; tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium;
Yield given. Multistep reaction;
DOI:10.1016/S0040-4020(01)89682-4
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) Ti(iPrO)4, 2.) NaIO4 / toluene / 2 h / Ambient temperature; 1.) THF, room temperature, 2 h, 2.) THF/water, 0 deg C, 1 h; room temperature, 2 h
2: BF3*OEt2 / CH2Cl2 / 0.2 h / -78 °C
3: H2, (Ph3P)3RhCl / benzene / Ambient temperature
With
titanium(IV) isopropylate; sodium periodate; Wilkinson's catalyst; boron trifluoride diethyl etherate; hydrogen;
In
dichloromethane; toluene; benzene;
DOI:10.1016/S0040-4020(01)89682-4
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) Ti(iPrO)4, 2.) NaIO4 / toluene / 2 h / Ambient temperature; 1.) THF, room temperature, 2 h, 2.) THF/water, 0 deg C, 1 h; room temperature, 2 h
2: BF3*OEt2 / CH2Cl2 / 0.2 h / -78 °C
With
titanium(IV) isopropylate; sodium periodate; boron trifluoride diethyl etherate;
In
dichloromethane; toluene;
DOI:10.1016/S0040-4020(01)89682-4
