Ethanone, 1-[5-(1,1-dimethylethyl)-2H-1,2,3-diazaphosphol-2-yl]-

Base Information

Chemical Name:Ethanone, 1-[5-(1,1-dimethylethyl)-2H-1,2,3-diazaphosphol-2-yl]-
CAS No.:137152-47-7
Molecular Formula:C₈H₁₃N₂OP
Molecular Weight:184.178
Hs Code.:
Mol file:137152-47-7.mol

Synonyms:Ethanone, 1-[5-(1,1-dimethylethyl)-2H-1,2,3-diazaphosphol-2-yl]-

Suppliers and Price of Ethanone, 1-[5-(1,1-dimethylethyl)-2H-1,2,3-diazaphosphol-2-yl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Ethanone, 1-[5-(1,1-dimethylethyl)-2H-1,2,3-diazaphosphol-2-yl]-

Chemical Property:

Boiling Point:86 - 88 °C (3 mmHg)
PSA：66.81000
LogP:1.28750

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Ethanone, 1-[5-(1,1-dimethylethyl)-2H-1,2,3-diazaphosphol-2-yl]-

There total 3 articles about Ethanone, 1-[5-(1,1-dimethylethyl)-2H-1,2,3-diazaphosphol-2-yl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 137152-44-4
1-(5-tert-Butyl-3-chloro-3,4-dihydro-[1,2,3]diazaphosphol-2-yl)-ethanone

: 137152-47-7
1-(5-tert-Butyl-[1,2,3]diazaphosphol-2-yl)-ethanone

Guidance literature:: With triethylamine; In benzene; for 8h;
DOI:10.1055/s-1991-26573

Reference yield: 52.0%

: 119393-10-1
Acetic acid [1,2,2-trimethyl-prop-(Z)-ylidene]-hydrazide

: 137152-47-7
1-(5-tert-Butyl-[1,2,3]diazaphosphol-2-yl)-ethanone

Guidance literature:: Acetic acid [1,2,2-trimethyl-prop-(Z)-ylidene]-hydrazide; With triethylamine; phosphorus trichloride; In dichloromethane; at 20 ℃;

With triethylamine; In benzene;
DOI:10.1002/jhet.5570430215

Reference yield:

: 119393-10-1
Acetic acid [1,2,2-trimethyl-prop-(Z)-ylidene]-hydrazide

: 137152-47-7
1-(5-tert-Butyl-[1,2,3]diazaphosphol-2-yl)-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / phosphorus trichloride, triethylamine / CH₂Cl₂ / 6 h / Ambient temperature

2: 75 percent / triethylamine / benzene / 8 h

With triethylamine; phosphorus trichloride; In dichloromethane; benzene;
DOI:10.1055/s-1991-26573