4-(6-Hydroxyhexyloxy)benzoic acid 4-methoxyphenyl ester

Base Information

• Chemical Name: 4-(6-Hydroxyhexyloxy)benzoic acid 4-methoxyphenyl ester
• CAS No.: 137407-31-9
• Molecular Formula: C20H24O5
• Molecular Weight: 344.408
• Hs Code.: 2918990090
• Mol file: 137407-31-9.mol

Synonyms:Hydroxyhexyloxybenzoicacidmethoxyphenylester;Benzoic acid, 4-[(6-hydroxyhexyl)oxy]-, 4-methoxyphenyl ester;4-Methoxyphenyl 4-[(6-hydroxyhexyl)oxy]benzoate;

Chemical Property of 4-(6-Hydroxyhexyloxy)benzoic acid 4-methoxyphenyl ester

Chemical Property:

• Melting Point: 100 °C
• Boiling Point: 517.252 °C at 760 mmHg
• Flash Point: 180.569 °C
• PSA: 64.99000
• Density: 1.145 g/cm³
• LogP: 3.84590

Purity/Quality:

98%,99%, ^*data from raw suppliers

4-Methoxyphenyl 4-(6-Hydroxyhexyloxy)benzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(6-Hydroxyhexyloxy)benzoic acid 4-methoxyphenyl ester

There total 5 articles about 4-(6-Hydroxyhexyloxy)benzoic acid 4-methoxyphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

1-bromo-6-hexanol (4286-55-9) + 4-hydroxybenzoic acid 4-methoxyphenyl ester (50687-62-2) → C20H24O5 (137407-31-9)

Guidance literature:

With potassium carbonate; In butanone; at 80 ℃; for 20h;

Reference yield:

4-methoxy-phenol (150-76-5) → C20H24O5 (137407-31-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid / benzene / 10 h / 100 °C

2: potassium carbonate / butanone / 20 h / 80 °C

With potassium carbonate; sulfuric acid; In butanone; benzene;

Reference yield:

4-hydroxy-benzoic acid (99-96-7) → C20H24O5 (137407-31-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid / benzene / 10 h / 100 °C

2: potassium carbonate / butanone / 20 h / 80 °C

With potassium carbonate; sulfuric acid; In butanone; benzene;

upstream raw materials:

1-iodohexan-6-ol

4-hydroxybenzoic acid 4-methoxyphenyl ester

4-methoxy-phenol

4-hydroxy-benzoic acid

Downstream raw materials:

C₂₂H₂₆O₇S

Refernces

• 1、 Nakamura, Naotake,Kagawa, Shinya. "Synthesis and physical properties of ferrocene derivatives (XXV) liquid crystallinity of 1,3-disubstituted ferrocene derivatives". experimental part. p. 150 - 159. Retrieved 2012/01/03.