1,4-Dioxa-8,9-diazaspiro[4.6]undec-8-ene

Base Information

Chemical Name:1,4-Dioxa-8,9-diazaspiro[4.6]undec-8-ene
CAS No.:138609-61-7
Molecular Formula:C7H12N2O2
Molecular Weight:0
Hs Code.:
DSSTox Substance ID:DTXSID30576546
Mol file:138609-61-7.mol

Synonyms:1,4-Dioxa-8,9-diazaspiro[4.6]undec-8-ene;138609-61-7;DTXSID30576546

Suppliers and Price of 1,4-Dioxa-8,9-diazaspiro[4.6]undec-8-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 1,4-Dioxa-8,9-diazaspiro[4.6]undec-8-ene

Chemical Property:

PSA：43.18000
LogP:-0.15330
XLogP3:0.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:156.089877630
Heavy Atom Count:11
Complexity:152

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CN=NCCC12OCCO2

Technology Process of 1,4-Dioxa-8,9-diazaspiro[4.6]undec-8-ene

There total 3 articles about 1,4-Dioxa-8,9-diazaspiro[4.6]undec-8-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 138609-57-1
1,4-Dioxa-8,9-diaza-spiro[4.6]undecane-8,9-dicarboxylic acid diallyl ester

: 138609-61-7
1,4-Dioxa-8,9-diaza-spiro[4.6]undec-8-ene

Guidance literature:: With N-butylamine; triphenylphosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; Ambient temperature;
DOI:10.1016/0040-4039(91)80240-7

Reference yield:

: 138609-57-1
1,4-Dioxa-8,9-diaza-spiro[4.6]undecane-8,9-dicarboxylic acid diallyl ester

: 138609-61-7
1,4-Dioxa-8,9-diaza-spiro[4.6]undec-8-ene

: 138609-59-3
8-Allyl-1,4-dioxa-8,9-diaza-spiro[4.6]undecane

Guidance literature:: With N-butylamine; triphenylphosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; Yield given. Yields of byproduct given; Ambient temperature;
DOI:10.1016/0040-4039(91)80240-7

Reference yield:

: 138609-57-1
1,4-Dioxa-8,9-diaza-spiro[4.6]undecane-8,9-dicarboxylic acid diallyl ester

: 138609-61-7
1,4-Dioxa-8,9-diaza-spiro[4.6]undec-8-ene

: 138609-59-3
8-Allyl-1,4-dioxa-8,9-diaza-spiro[4.6]undecane

: 138609-60-6
9-Allyl-1,4-dioxa-8,9-diaza-spiro[4.6]undec-7-ene

Guidance literature:: With N-butylamine; triphenylphosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; Product distribution; Ambient temperature; or in BuNH₂;
DOI:10.1016/0040-4039(91)80240-7