4-Methoxyphenyl 3-O-Benzyl-2-deoxy-2-phthalimido-beta-D-glucopyranoside

Base Information

Chemical Name:4-Methoxyphenyl 3-O-Benzyl-2-deoxy-2-phthalimido-beta-D-glucopyranoside
CAS No.:138906-44-2
Molecular Formula:C28H27NO8
Molecular Weight:505.52
Hs Code.:
DSSTox Substance ID:DTXSID50693668
Wikidata:Q82622678
Mol file:138906-44-2.mol

Synonyms:138906-44-2;4-Methoxyphenyl 3-O-Benzyl-2-deoxy-2-phthalimido-beta-D-glucopyranoside;2-[(2S,3R,4R,5S,6R)-5-hydroxy-6-(hydroxymethyl)-2-(4-methoxyphenoxy)-4-phenylmethoxyoxan-3-yl]isoindole-1,3-dione;beta-D-Glucopyranoside, 4-methoxyphenyl 2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-3-O-(phenylmethyl)-;SCHEMBL3628586;DTXSID50693668;ZWFNEOGZZUQQDV-JWJHGQTKSA-N;M1610;4-Methoxyphenyl 3-O-benzyl-2-deoxy-2-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-beta-D-glucopyranoside

Suppliers and Price of 4-Methoxyphenyl 3-O-Benzyl-2-deoxy-2-phthalimido-beta-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chem-Impex
4-Methoxyphenyl3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside,≥98% ≥98%
1G
$ 454.27

Biosynth Carbosynth
4-Methoxyphenyl 3-O-benzyl-2-deoxy-2-phthalimido-b-D-glucopyranoside
50 g
$ 150.00

Biosynth Carbosynth
4-Methoxyphenyl 3-O-benzyl-2-deoxy-2-phthalimido-b-D-glucopyranoside
25 g
$ 88.00

Biosynth Carbosynth
4-Methoxyphenyl 3-O-benzyl-2-deoxy-2-phthalimido-b-D-glucopyranoside
10 g
$ 44.00

Biosynth Carbosynth
4-Methoxyphenyl 3-O-benzyl-2-deoxy-2-phthalimido-b-D-glucopyranoside
100 g
$ 255.00

Biosynth Carbosynth
4-Methoxyphenyl 3-O-benzyl-2-deoxy-2-phthalimido-b-D-glucopyranoside
250 g
$ 510.00

American Custom Chemicals Corporation
4-METHOXYPHENYL 3-O-BENZYL-2-DEOXY-2-PHTHALIMIDO-BETA-D-GLUCOPYRANOSIDE 95.00%
5MG
$ 501.44

AK Scientific
4-Methoxyphenyl3-O-benzyl-2-deoxy-2-phthalimido-beta-D-glucopyranoside
25g
$ 168.00

Total 3 raw suppliers

Chemical Property of 4-Methoxyphenyl 3-O-Benzyl-2-deoxy-2-phthalimido-beta-D-glucopyranoside

Chemical Property:

Refractive Index:1.668
PSA：114.76000
LogP:2.34020
Storage Temp.:Freezer
XLogP3:3.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:8
Exact Mass:505.17366682
Heavy Atom Count:37
Complexity:756

Purity/Quality:

95% ^*data from raw suppliers

4-Methoxyphenyl3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside,≥98% ≥98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)OC2C(C(C(C(O2)CO)O)OCC3=CC=CC=C3)N4C(=O)C5=CC=CC=C5C4=O
Isomeric SMILES:COC1=CC=C(C=C1)O[C@H]2[C@@H]([C@H]([C@@H]([C@H](O2)CO)O)OCC3=CC=CC=C3)N4C(=O)C5=CC=CC=C5C4=O

Technology Process of 4-Methoxyphenyl 3-O-Benzyl-2-deoxy-2-phthalimido-beta-D-glucopyranoside

There total 5 articles about 4-Methoxyphenyl 3-O-Benzyl-2-deoxy-2-phthalimido-beta-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 129575-88-8
p-Methoxyphenyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 138906-44-2
para-MethoxyPhenyl 3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With toluene-4-sulfonic acid; In 1,4-dioxane; methanol; 1) 1 h, 60 deg C, 2) 45 min, 85 deg C;
DOI:10.1016/0008-6215(93)84080-P

Reference yield:

: 10022-13-6
1,3,4,6-tetra-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranose

: 138906-44-2
para-MethoxyPhenyl 3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / Me₃SiOTf / 1,2-dichloro-ethane / 3 h / 0 °C

2: p-TsOH*H₂O / dimethylformamide / 20 h / 20 °C

3: 61 percent / NaH / dimethylformamide / 20 h / 20 °C

4: 77 percent / p-TsOH*H₂O / methanol; dioxane / 1) 1 h, 60 deg C, 2) 45 min, 85 deg C

With trimethylsilyl trifluoromethanesulfonate; sodium hydride; toluene-4-sulfonic acid; In 1,4-dioxane; methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(93)84080-P

Reference yield:

: 138906-43-1
4-methoxyphenyl 4,6-di-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 138906-44-2
para-MethoxyPhenyl 3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / NaH / dimethylformamide / 20 h / 20 °C

2: 77 percent / p-TsOH*H₂O / methanol; dioxane / 1) 1 h, 60 deg C, 2) 45 min, 85 deg C

With sodium hydride; toluene-4-sulfonic acid; In 1,4-dioxane; methanol; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(93)84080-P