1,4-Dioxin-2-carbonyl chloride, 5,6-dihydro-3-methyl- (9CI)

Base Information

Chemical Name:1,4-Dioxin-2-carbonyl chloride, 5,6-dihydro-3-methyl- (9CI)
CAS No.:139035-98-6
Molecular Formula:C6H7ClO3
Molecular Weight:162.57098
Hs Code.:
Mol file:139035-98-6.mol

Synonyms:1,4-Dioxin-2-carbonyl chloride, 5,6-dihydro-3-methyl- (9CI)

Suppliers and Price of 1,4-Dioxin-2-carbonyl chloride, 5,6-dihydro-3-methyl- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 1,4-Dioxin-2-carbonyl chloride, 5,6-dihydro-3-methyl- (9CI)

Chemical Property:

PSA：35.53000
LogP:1.03010

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,4-Dioxin-2-carbonyl chloride, 5,6-dihydro-3-methyl- (9CI)

There total 3 articles about 1,4-Dioxin-2-carbonyl chloride, 5,6-dihydro-3-methyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3973-22-6
5-methyl-2,3-dihydro-[1,4]dioxine

: 139035-98-6
3-Methyl-5,6-dihydro-[1,4]dioxine-2-carbonyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 33.3 percent / pyridine / CH₂Cl₂ / 24 h / Ambient temperature

2: 69 percent / KOH / toluene / 7 h / Heating

3: SOCl₂ / 1.5 h / Heating

With pyridine; potassium hydroxide; thionyl chloride; In dichloromethane; toluene;
DOI:10.1021/jf970960d

Reference yield:

: 135813-43-3
1-(5,6-dihydro-3-methyl-1,4-dioxin-2-yl)-2,2,2-trifluoroethanone

: 139035-98-6
3-Methyl-5,6-dihydro-[1,4]dioxine-2-carbonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / KOH / toluene / 7 h / Heating

2: SOCl₂ / 1.5 h / Heating

With potassium hydroxide; thionyl chloride; In toluene;
DOI:10.1021/jf970960d