1-Aza-2,5-disilacyclopentane-1-acetic acid, -alpha-,2,2,5,5-pentamethyl-, phenylmethyl ester, (S)- (9CI)

Base Information

Chemical Name:1-Aza-2,5-disilacyclopentane-1-acetic acid, -alpha-,2,2,5,5-pentamethyl-, phenylmethyl ester, (S)- (9CI)
CAS No.:139215-48-8
Molecular Formula:C₁₆H₂₇NO₂Si₂
Molecular Weight:321.567
Hs Code.:

Synonyms:1-Aza-2,5-disilacyclopentane-1-acetic acid, -alpha-,2,2,5,5-pentamethyl-, phenylmethyl ester, (S)- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Aza-2,5-disilacyclopentane-1-acetic acid, -alpha-,2,2,5,5-pentamethyl-, phenylmethyl ester, (S)- (9CI)

Chemical Property:

PSA：29.54000
LogP:3.78200

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 1-Aza-2,5-disilacyclopentane-1-acetic acid, -alpha-,2,2,5,5-pentamethyl-, phenylmethyl ester, (S)- (9CI)

There total 2 articles about 1-Aza-2,5-disilacyclopentane-1-acetic acid, -alpha-,2,2,5,5-pentamethyl-, phenylmethyl ester, (S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 13528-93-3
1,2-bis-(chlorodimethylsilyl)ethane

: 5557-81-3,5557-83-5,34404-37-0
L-alanine benzyl ester hydrochloride

: 139215-48-8
(S)-2-(2,2,5,5-Tetramethyl-[1,2,5]azadisilolidin-1-yl)-propionic acid benzyl ester

Guidance literature:: With triethylamine; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1016/S0040-4020(01)80720-1

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 139215-48-8
(S)-2-(2,2,5,5-Tetramethyl-[1,2,5]azadisilolidin-1-yl)-propionic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

2: 60 percent / triethylamine / CH₂Cl₂ / 24 h / Ambient temperature

With triethylamine; In dichloromethane;
DOI:10.1016/S0040-4020(01)80720-1