1-Aza-2,5-disilacyclopentane-1-acetic acid, -alpha-,2,2,5,5-pentamethyl-, 2-(trimethylsilyl)ethyl ester, (S)- (9CI)

Base Information

Chemical Name:1-Aza-2,5-disilacyclopentane-1-acetic acid, -alpha-,2,2,5,5-pentamethyl-, 2-(trimethylsilyl)ethyl ester, (S)- (9CI)
CAS No.:139215-49-9
Molecular Formula:C14H33NO2Si3
Molecular Weight:331.68
Hs Code.:

Synonyms:1-Aza-2,5-disilacyclopentane-1-acetic acid, -alpha-,2,2,5,5-pentamethyl-, 2-(trimethylsilyl)ethyl ester, (S)- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Aza-2,5-disilacyclopentane-1-acetic acid, -alpha-,2,2,5,5-pentamethyl-, 2-(trimethylsilyl)ethyl ester, (S)- (9CI)

Chemical Property:

PSA：29.54000
LogP:3.92000

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 1-Aza-2,5-disilacyclopentane-1-acetic acid, -alpha-,2,2,5,5-pentamethyl-, 2-(trimethylsilyl)ethyl ester, (S)- (9CI)

There total 2 articles about 1-Aza-2,5-disilacyclopentane-1-acetic acid, -alpha-,2,2,5,5-pentamethyl-, 2-(trimethylsilyl)ethyl ester, (S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 13528-93-3
1,2-bis-(chlorodimethylsilyl)ethane

: 103225-23-6
(S)-Alanin-(2-trimethylsilylethyl)ester

: 139215-49-9
(S)-2-(2,2,5,5-Tetramethyl-[1,2,5]azadisilolidin-1-yl)-propionic acid 2-trimethylsilanyl-ethyl ester

Guidance literature:: With triethylamine; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1016/S0040-4020(01)80720-1

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 139215-49-9
(S)-2-(2,2,5,5-Tetramethyl-[1,2,5]azadisilolidin-1-yl)-propionic acid 2-trimethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

2: 69 percent / triethylamine / CH₂Cl₂ / 24 h / Ambient temperature

With triethylamine; In dichloromethane;
DOI:10.1016/S0040-4020(01)80720-1