Carbonochloridimidothioicacid, (4-nitrophenyl)-, anhydrosulfide with thiohypochlorous acid (9CI)

Base Information

• Chemical Name: Carbonochloridimidothioicacid, (4-nitrophenyl)-, anhydrosulfide with thiohypochlorous acid (9CI)
• CAS No.: 5180-21-2
• Molecular Formula: C₇H₄Cl₂N₂O₂S
• Molecular Weight: 251.093

Synonyms:Formimidoylchloride, 1-(chlorothio)-N-(p-nitrophenyl)- (7CI,8CI)

Chemical Property of Carbonochloridimidothioicacid, (4-nitrophenyl)-, anhydrosulfide with thiohypochlorous acid (9CI)

Chemical Property:

Purity/Quality:

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Technology Process of Carbonochloridimidothioicacid, (4-nitrophenyl)-, anhydrosulfide with thiohypochlorous acid (9CI)

There total 2 articles about Carbonochloridimidothioicacid, (4-nitrophenyl)-, anhydrosulfide with thiohypochlorous acid (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-nitrophenyl isothiocyanate (2131-61-5) → hypochlorous N-(4-nitro-phenyl)-carbonochloridimidic thioanhydride (5180-21-2)

Guidance literature:

With chlorine; In chloroform;

DOI:10.1021/jo01341a046

Reference yield:

→ C7H4Cl2N2O2S (5180-21-2)

Guidance literature:

RNCS, Cl2;

Reference yield:

hypochlorous N-(4-nitro-phenyl)-carbonochloridimidic thioanhydride (5180-21-2) + N′-(4-bromophenyl)benzamidine (21719-91-5) → [4-(4-bromo-phenyl)-3-phenyl-4H-[1,2,4]thiadiazol-5-ylidene]-(4-nitro-phenyl)-amine (33863-70-6)

Guidance literature:

In benzene;

DOI:10.1016/S0040-4020(01)98142-6

upstream raw materials:

p-nitrophenyl isothiocyanate

Downstream raw materials:

(3,4-diphenyl-4H-[1,2,4]thiadiazol-5-ylidene)-(4-nitro-phenyl)-amine

[4-(4-bromo-phenyl)-3-phenyl-4H-[1,2,4]thiadiazol-5-ylidene]-(4-nitro-phenyl)-amine

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