Technology Process of 2-Azabicyclo[2.2.1]heptan-6-ol,acetate(ester),(1R-exo)-(9CI)
There total 3 articles about 2-Azabicyclo[2.2.1]heptan-6-ol,acetate(ester),(1R-exo)-(9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium formate;
palladium on activated charcoal;
In
methanol;
for 1h;
Yield given;
Heating;
DOI:10.1021/jm00090a006
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) 1M BH3*THF, 2.) NaOH, 50percent H2O2 / 1.) THF, 0-10 deg C, 2 h, 2.) THF, H2O, 35-40 deg C, 1.5 h
2: 90 percent / Et3N, DMAP / CH2Cl2 / Ambient temperature
3: HCO2NH4 / Pd/C / methanol / 1 h / Heating
With
dmap; sodium hydroxide; borane-THF; dihydrogen peroxide; ammonium formate; triethylamine;
palladium on activated charcoal;
In
methanol; dichloromethane;
DOI:10.1021/jm00090a006
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 90 percent / Et3N, DMAP / CH2Cl2 / Ambient temperature
2: HCO2NH4 / Pd/C / methanol / 1 h / Heating
With
dmap; ammonium formate; triethylamine;
palladium on activated charcoal;
In
methanol; dichloromethane;
DOI:10.1021/jm00090a006
