1H-Imidazole-4-carboxylicacid,2-amino-5-cyano-1-methyl-,ethylester(9CI)

Base Information

Chemical Name:1H-Imidazole-4-carboxylicacid,2-amino-5-cyano-1-methyl-,ethylester(9CI)
CAS No.:146091-72-7
Molecular Formula:C₈H₁₀N₄O₂
Molecular Weight:194.193
Hs Code.:
Mol file:146091-72-7.mol

Synonyms:1H-Imidazole-4-carboxylicacid,2-amino-5-cyano-1-methyl-,ethylester(9CI)

Suppliers and Price of 1H-Imidazole-4-carboxylicacid,2-amino-5-cyano-1-methyl-,ethylester(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 1H-Imidazole-4-carboxylicacid,2-amino-5-cyano-1-methyl-,ethylester(9CI)

Chemical Property:

PSA：94.66000
LogP:-0.01922

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-Imidazole-4-carboxylicacid,2-amino-5-cyano-1-methyl-,ethylester(9CI)

There total 2 articles about 1H-Imidazole-4-carboxylicacid,2-amino-5-cyano-1-methyl-,ethylester(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77-78-1
dimethyl sulfate

: 75877-59-7
ethyl 2-amino-4⁽⁵⁾-cyano-5⁽⁴⁾-imidazolecarboxylate

: 146091-72-7
ethyl 2-amino-5-cyano-1-methyl-4-imidazolecarboxylate

: 146091-70-5
ethyl 2-amino-4-cyano-1-methyl-5-imidazolecarboxylate

Guidance literature:: With sodium hydride; In hexane; N,N-dimethyl-formamide; at 0 - 21 ℃; for 12h;
DOI:10.1016/S0040-4020(01)86980-5

Reference yield:

: 40953-34-2
2-amino-1H-imidazole-4,5-dicarbonitrile

: 146091-72-7
ethyl 2-amino-5-cyano-1-methyl-4-imidazolecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 37 percent / conc. sulphuric acid / 10 h / Heating

2: 60percent sodium hydride in mineral oil / dimethylformamide; hexane / 12 h / 0 - 21 °C

With sulfuric acid; sodium hydride; In hexane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)86980-5