1,6-DI-O-ACETYL-2,3-ISOPROPYLIDENE-D-RIBOSE

Base Information

Chemical Name:1,6-DI-O-ACETYL-2,3-ISOPROPYLIDENE-D-RIBOSE
CAS No.:141979-56-8
Molecular Formula:C12H18 O7
Molecular Weight:274.27
Hs Code.:
Mol file:141979-56-8.mol

Synonyms:Furo[3,4-d]-1,3-dioxole,D-ribofuranose deriv.

Suppliers and Price of 1,6-DI-O-ACETYL-2,3-ISOPROPYLIDENE-D-RIBOSE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Usbiological
1,5-Di-O-acetyl-2,3-O-isopropylidene-D-ribofuranose
1g
$ 329.00

TRC
1,5-Di-O-acetyl-2,3-isopropylidene-D-ribose
5g
$ 150.00

TRC
1,5-Di-O-acetyl-2,3-isopropylidene-D-ribose
1g
$ 55.00

TRC
1,5-Di-O-acetyl-2,3-isopropylidene-D-ribose
2g
$ 90.00

Biosynth Carbosynth
1,5-Di-O-acetyl-2,3-O-isopropylidene-D-ribofuranose
2 g
$ 90.00

Biosynth Carbosynth
1,5-Di-O-acetyl-2,3-O-isopropylidene-D-ribofuranose
1 g
$ 55.00

Biosynth Carbosynth
1,5-Di-O-acetyl-2,3-O-isopropylidene-D-ribofuranose
5 g
$ 190.00

Biosynth Carbosynth
1,5-Di-O-acetyl-2,3-O-isopropylidene-D-ribofuranose
10 g
$ 350.00

Biosynth Carbosynth
1,5-Di-O-acetyl-2,3-O-isopropylidene-D-ribofuranose
25 g
$ 800.00

American Custom Chemicals Corporation
1,5-DI-O-ACETYL-2,3-O-ISOPROPYLIDENE-D-RIBOFURANOSE 95.00%
1G
$ 480.00

Total 7 raw suppliers

Chemical Property of 1,6-DI-O-ACETYL-2,3-ISOPROPYLIDENE-D-RIBOSE

Chemical Property:

Vapor Pressure:9.28E-05mmHg at 25°C
Refractive Index:1.485
Boiling Point:119°C@0.1mmHg
Flash Point:147.5°C
PSA：80.29000
Density:1.26g/cm³
LogP:0.35760
Storage Temp.:Refrigerator
Solubility.:Chloroform (Slightly), Ethyl Acetate (Slightly)

Purity/Quality:

98%,99%, ^*data from raw suppliers

1,5-Di-O-acetyl-2,3-O-isopropylidene-D-ribofuranose ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 1,5-Di-O-acetyl-2,3-isopropylidene-D-ribose (cas# 141979-56-8) is a compound useful in organic synthesis.

Technology Process of 1,6-DI-O-ACETYL-2,3-ISOPROPYLIDENE-D-RIBOSE

There total 2 articles about 1,6-DI-O-ACETYL-2,3-ISOPROPYLIDENE-D-RIBOSE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 67814-68-0,70266-87-4,76249-50-8,76249-51-9,93451-15-1,4099-88-1
2,3-O-isopropylidene-D-ribofuranose

: 108-24-7
acetic anhydride

: 141979-56-8
1,5-O-diacetyl-2,3-O-isopropylidene-D-ribofuranoside

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1021/ja020238i

Reference yield:

: 532-20-7,613-83-2,7261-25-8,7687-39-0,13221-22-2,14795-83-6,15761-67-8,20074-49-1,25545-03-3,25545-04-4,32445-75-3,34436-17-4,36441-93-7,36468-53-8,37110-85-3,37388-49-1,38029-69-5,40461-77-6,40461-89-0,41546-19-4,41546-20-7,41546-21-8,41546-26-3,41546-29-6,41546-30-9,41546-31-0,126872-16-0,131064-98-7
D-Ribose

: 141979-56-8
1,5-O-diacetyl-2,3-O-isopropylidene-D-ribofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: H(+)

2: pyridine

With hydrogen cation; In pyridine;
DOI:10.1016/S0040-4039(01)01446-0

Reference yield:

: 141979-56-8
1,5-O-diacetyl-2,3-O-isopropylidene-D-ribofuranoside

: 442913-67-9
(S)-2-(4-Methoxy-benzyloxy)-hex-5-enoic acid (S)-1-((4S,5R)-2,2-dimethyl-5-vinyl-[1,3]dioxolan-4-yl)-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: TMSOTf / acetonitrile / 24 h / 0 °C

1.2: H₂ / Pd/C / CH₂Cl₂ / 3 h / 20 °C / 760.05 Torr

2.1: 380 mg / MeONa / methanol / 4 h / 20 °C

3.1: 89 percent / iodine; PPh₃; imidazole / CH₂Cl₂ / 20 h / 20 °C

4.1: 86 percent / Zn(Ag)-graphite / tetrahydrofuran / 0.5 h / 20 °C

5.1: 87 percent / DCC; DMAP / CH₂Cl₂ / 28 h / 20 °C

With 1H-imidazole; dmap; trimethylsilyl trifluoromethanesulfonate; iodine; sodium methylate; dicyclohexyl-carbodiimide; triphenylphosphine; silver; zinc; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;
DOI:10.1021/ja020238i