Cyclopenta[b]pyrrole-6-methanol, octahydro-1-methyl-, [3aS-(3a-alpha-,6-alpha-,6a-alpha-)]- (9CI)

Base Information

Chemical Name:Cyclopenta[b]pyrrole-6-methanol, octahydro-1-methyl-, [3aS-(3a-alpha-,6-alpha-,6a-alpha-)]- (9CI)
CAS No.:142321-08-2
Molecular Formula:C₉H₁₇NO
Molecular Weight:155.24
Hs Code.:
Mol file:142321-08-2.mol

Synonyms:Cyclopenta[b]pyrrole-6-methanol, octahydro-1-methyl-, [3aS-(3a-alpha-,6-alpha-,6a-alpha-)]- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclopenta[b]pyrrole-6-methanol, octahydro-1-methyl-, [3aS-(3a-alpha-,6-alpha-,6a-alpha-)]- (9CI)

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Technology Process of Cyclopenta[b]pyrrole-6-methanol, octahydro-1-methyl-, [3aS-(3a-alpha-,6-alpha-,6a-alpha-)]- (9CI)

There total 13 articles about Cyclopenta[b]pyrrole-6-methanol, octahydro-1-methyl-, [3aS-(3a-alpha-,6-alpha-,6a-alpha-)]- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 142321-07-1,142433-91-8,142433-92-9,142433-96-3
(1R^*,5S^*,8R^*)-2-Methyl-3-oxo-2-azabicyclo<3.3.0>octan-8-carbonsaeure-methylester

: 142321-08-2,142433-97-4,142434-08-0
(1R^*,5S^*,8R^*)-8-(Hydroxymethyl)-2-methyl-2-azabicyclo<3.3.0>octan

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 2h; Ambient temperature;

Reference yield:

: 142320-97-6,142433-88-3
(1R^*,2R^*,5R^*,8S^*)-2-(Dimethylamino)-8-(methylamino)bicyclo<3.2.1>octan

: 142321-08-2,142433-97-4,142434-08-0
(1R^*,5S^*,8R^*)-8-(Hydroxymethyl)-2-methyl-2-azabicyclo<3.3.0>octan

Guidance literature:: Multi-step reaction with 7 steps

1: 78 percent / CH₂Cl₂ / 16 h / Ambient temperature

2: 30percent H₂O₂ / methanol / 72 h

3: 3 h / 120 °C

5: H₂ / 10percent Pd-C / methanol

6: NaOCH₃ / methanol

7: 73 percent / LiAlH₄ / diethyl ether / 2 h / Ambient temperature

With lithium aluminium tetrahydride; hydrogen; dihydrogen peroxide; sodium methylate; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane;

Reference yield:

: 142321-02-6,142506-82-9
(1R^*,5S^*,8R^*)-8-<(Benzyloxycarbonyl)methylamino>bicyclo<3.2.1>oct-2-en

: 142321-08-2,142433-97-4,142434-08-0
(1R^*,5S^*,8R^*)-8-(Hydroxymethyl)-2-methyl-2-azabicyclo<3.3.0>octan

Guidance literature:: Multi-step reaction with 4 steps

2: H₂ / 10percent Pd-C / methanol

3: NaOCH₃ / methanol

4: 73 percent / LiAlH₄ / diethyl ether / 2 h / Ambient temperature

With lithium aluminium tetrahydride; hydrogen; sodium methylate; palladium on activated charcoal; In methanol; diethyl ether;