8-Oxabicyclo[3.2.1]oct-6-en-3-one,2-(1-methylethyl)-,(1R,2S,5R)-rel-(9CI)

Base Information

Chemical Name:8-Oxabicyclo[3.2.1]oct-6-en-3-one,2-(1-methylethyl)-,(1R,2S,5R)-rel-(9CI)
CAS No.:147729-86-0
Molecular Formula:C₁₀H₁₄O₂
Molecular Weight:166.22
Hs Code.:
Mol file:147729-86-0.mol

Synonyms:8-Oxabicyclo[3.2.1]oct-6-en-3-one,2-(1-methylethyl)-, endo-(?à)-; 8-Oxabicyclo[3.2.1]oct-6-en-3-one, 2-(1-methylethyl)-, endo-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-Oxabicyclo[3.2.1]oct-6-en-3-one,2-(1-methylethyl)-,(1R,2S,5R)-rel-(9CI)

Chemical Property:

PSA：26.30000
LogP:1.55500

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 8-Oxabicyclo[3.2.1]oct-6-en-3-one,2-(1-methylethyl)-,(1R,2S,5R)-rel-(9CI)

There total 6 articles about 8-Oxabicyclo[3.2.1]oct-6-en-3-one,2-(1-methylethyl)-,(1R,2S,5R)-rel-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2,4-dichloro-2-isopropyl-8-oxabicyclo[3.2.1]-oct-6-en-3-one

: 147729-86-0
endo-2-isopropyl-8-oxabicyclo[3.2.1]oct-6-en-3-one

Guidance literature:: With zinc/copper couple; ammonium chloride; In methanol; for 24h;
DOI:10.1002/ejoc.200500070

Reference yield:

: 25328-92-1
1,1,1-trichloro-4-methyl-2-pentanone

: 147729-86-0
endo-2-isopropyl-8-oxabicyclo[3.2.1]oct-6-en-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: lithium perchlorate; triethylamine / diethyl ether / 48 h / 20 °C

2: 0.1 g / ammonium chloride; zinc*copper / methanol / 24 h

With zinc/copper couple; ammonium chloride; lithium perchlorate; triethylamine; In methanol; diethyl ether;
DOI:10.1002/ejoc.200500070

Reference yield:

: 110-00-9
furan

: 1578-06-9
1,1,3-tribromo-4-methylpentan-2-one

: 66365-97-7,147729-86-0
2-isopropyl-8-oxa-bicyclo[3.2.1]oct-6-en-3-one

Guidance literature:: With diiron nonacarbonyl; copper; ammonium chloride; zinc; Yield given. Multistep reaction; 1.) benzene, reflux, 16 h; 2.) MeOH, r.t., 1.5 h;
DOI:10.1016/S0040-4020(01)91427-9