4(1H)-Quinolinone, 3,3-dichloro-2,3-dihydro-2-hydroxy-6-methyl-2-phenyl-

Base Information

Chemical Name:4(1H)-Quinolinone, 3,3-dichloro-2,3-dihydro-2-hydroxy-6-methyl-2-phenyl-
CAS No.:147779-27-9
Molecular Formula:C₁₆H₁₃Cl₂NO₂
Molecular Weight:322.191
Hs Code.:
Mol file:147779-27-9.mol

Synonyms:4(1H)-Quinolinone, 3,3-dichloro-2,3-dihydro-2-hydroxy-6-methyl-2-phenyl-

Suppliers and Price of 4(1H)-Quinolinone, 3,3-dichloro-2,3-dihydro-2-hydroxy-6-methyl-2-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 4(1H)-Quinolinone, 3,3-dichloro-2,3-dihydro-2-hydroxy-6-methyl-2-phenyl-

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4(1H)-Quinolinone, 3,3-dichloro-2,3-dihydro-2-hydroxy-6-methyl-2-phenyl-

There total 4 articles about 4(1H)-Quinolinone, 3,3-dichloro-2,3-dihydro-2-hydroxy-6-methyl-2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 117039-84-6
3-chloro-6-methyl-2-phenyl-4(1H)-quinolinone

: 147779-27-9
3,3-dichloro-2,3-dihydro-2-hydroxy-6-methyl-2-phenylquinolin-4(1H)-one

Guidance literature:: Multi-step reaction with 5 steps

1: 66 percent / sodium dichloroisocyanurate, aq. NaOH / 1.5 h

2: 15 mg / 2 M HCl / acetone / 30 h / also with aq. NaOH in MeOH

3: 66 percent / sodium dichloroisocyanurate, aq. NaOH / methanol

4: 75 mg / conc. H₂SO₄ / 1 h / Ambient temperature

5: H₂O / acetone

With hydrogenchloride; sodium hydroxide; sulfuric acid; water; sode de l'acide trichloroisocyanurique; In methanol; acetone;
DOI:10.1039/P19930000511

Reference yield:

: 147779-28-0
3,3-dichloro-2,3-dihydro-2-methoxy-6-methyl-2-phenylquinolin-4(1H)-one

: 147779-27-9
3,3-dichloro-2,3-dihydro-2-hydroxy-6-methyl-2-phenylquinolin-4(1H)-one

Guidance literature:: Multi-step reaction with 4 steps

1: 15 mg / 2 M HCl / acetone / 30 h / also with aq. NaOH in MeOH

2: 66 percent / sodium dichloroisocyanurate, aq. NaOH / 1.5 h

3: 75 mg / conc. H₂SO₄ / 1 h / Ambient temperature

4: H₂O / acetone

With hydrogenchloride; sodium hydroxide; sulfuric acid; water; sode de l'acide trichloroisocyanurique; In acetone;
DOI:10.1039/P19930000511

Reference yield:

: 15104-17-3
2-phenyl-6-methyl-1,4-dihydro-4-oxoquinoline

: 147779-27-9
3,3-dichloro-2,3-dihydro-2-hydroxy-6-methyl-2-phenylquinolin-4(1H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / sodium dichloroisocyanurate, aq. NaOH / 0.17 h

2: 75 mg / conc. H₂SO₄ / 1 h / Ambient temperature

3: H₂O / acetone

With sodium hydroxide; sulfuric acid; water; sode de l'acide trichloroisocyanurique; In acetone;
DOI:10.1039/P19930000511