3-Oxabicyclo[3.1.0]hexane-2,4-dione,1-(1-methylethyl)-,(1R)-(9CI)

Base Information

Chemical Name:3-Oxabicyclo[3.1.0]hexane-2,4-dione,1-(1-methylethyl)-,(1R)-(9CI)
CAS No.:148261-91-0
Molecular Formula:C₈H₁₀O₃
Molecular Weight:154.166
Hs Code.:
Mol file:148261-91-0.mol

Synonyms:3-Oxabicyclo[3.1.0]hexane-2,4-dione,1-(1-methylethyl)-,(1R)-(9CI)

Suppliers and Price of 3-Oxabicyclo[3.1.0]hexane-2,4-dione,1-(1-methylethyl)-,(1R)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-Oxabicyclo[3.1.0]hexane-2,4-dione,1-(1-methylethyl)-,(1R)-(9CI)

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-Oxabicyclo[3.1.0]hexane-2,4-dione,1-(1-methylethyl)-,(1R)-(9CI)

There total 6 articles about 3-Oxabicyclo[3.1.0]hexane-2,4-dione,1-(1-methylethyl)-,(1R)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 513-18-8,702-88-5,702-89-6,148261-92-1
(+/-)-1-isopropyl-cyclopropane-1r,2t-dicarboxylic acid

: 875-16-1,73127-02-3,148261-91-0
(+/-)-1-isopropyl-cyclopropane-1r,2c-dicarboxylic acid-anhydride

Guidance literature:: With acetic anhydride; at 220 ℃;
DOI:10.1039/jr9360000828

Reference yield:

: 68834-46-8
ethyl α-isopropylacrylate

: 875-16-1,73127-02-3,148261-91-0
(+/-)-1-isopropyl-cyclopropane-1r,2c-dicarboxylic acid-anhydride

Guidance literature:: Multi-step reaction with 2 steps

1: Erhitzen des Reaktionsprodukts auf 200grad und Erhitzen des erhaltenen Ester-Gemisches mit wss.-methanol. Kalilauge oder mit aethanol. Kalilauge

2: acetyl chloride / 180 °C

With acetyl chloride;

Reference yield:

: 609-12-1
ethyl 2-bromoisovalerate

: 875-16-1,73127-02-3,148261-91-0
(+/-)-1-isopropyl-cyclopropane-1r,2c-dicarboxylic acid-anhydride

Guidance literature:: Multi-step reaction with 2 steps

1: NaNH₂ / Hydrolysieren des Reaktionsprodukts

2: acetyl chloride / 220 °C

With sodium amide; acetyl chloride;