Ethanehydrazonoylchloride, 2-[(2-chlorophenyl)amino]-2-oxo-N-phenyl-

Base Information

Chemical Name:Ethanehydrazonoylchloride, 2-[(2-chlorophenyl)amino]-2-oxo-N-phenyl-
CAS No.:148367-97-9
Molecular Formula:C₁₄H₁₁Cl₂N₃O
Molecular Weight:308.167
Hs Code.:2928000090
DSSTox Substance ID:DTXSID70375696
Mol file:148367-97-9.mol

Synonyms:Ethanehydrazonoylchloride, 2-[(2-chlorophenyl)amino]-2-oxo-N-phenyl-;148367-97-9;2-(2-chloroanilino)-2-oxo-N-phenylethanehydrazonoyl chloride;(1E)-2-[(2-Chlorophenyl)amino]-2-oxo-N-phenylethanehydrazonoyl chloride;DTXSID70375696;BCP26151;(E)-2-(2-chlorophenylamino)-2-oxo-N'-phenylacetohydrazonoyl chloride;2-Chloro-2-(2-phenylhydrazono)-N-(2-chlorophenyl)-;2-Chloro-2-(2-phenylhydrazono)-N-(2-chlorophenyl)-acetamide;acetamide

Suppliers and Price of Ethanehydrazonoylchloride, 2-[(2-chlorophenyl)amino]-2-oxo-N-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2-((2-Chlorophenyl)amino)-2-oxo-N'-phenylacetohydrazonoylchloride 97%
250mg
$ 336.00

American Custom Chemicals Corporation
2-CHLORO-2-(2-PHENYLHYDRAZONO)-N-(2-CHLOROPHENYL)-ACETAMIDE 95.00%
5MG
$ 503.98

Total 7 raw suppliers

Chemical Property of Ethanehydrazonoylchloride, 2-[(2-chlorophenyl)amino]-2-oxo-N-phenyl-

Chemical Property:

Refractive Index:1.62
PKA:8.27±0.70(Predicted)
PSA：53.49000
Density:1.33g/cm³
LogP:4.08890
XLogP3:5.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:307.0279174
Heavy Atom Count:20
Complexity:356

Purity/Quality:

97% ^*data from raw suppliers

2-((2-Chlorophenyl)amino)-2-oxo-N'-phenylacetohydrazonoylchloride 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)NN=C(C(=O)NC2=CC=CC=C2Cl)Cl

Technology Process of Ethanehydrazonoylchloride, 2-[(2-chlorophenyl)amino]-2-oxo-N-phenyl-

There total 3 articles about Ethanehydrazonoylchloride, 2-[(2-chlorophenyl)amino]-2-oxo-N-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 31009-93-5
2-chloro-N-(2-chlorophenyl)-3-oxobutanamide

: 62-53-3
aniline

: 463342-71-4,148367-97-9
(1Z)-2-[(2-chlorophenyl)amino]-2-oxo-N-phenylethanehydrazonoyl chloride

Guidance literature:: aniline; With hydrogenchloride; sodium nitrite; In water; at 0 - 5 ℃;

2-chloro-N-(2-chlorophenyl)-3-oxobutanamide; With sodium acetate; In methanol; water; at 5 - 10 ℃; for 2h; Further stages.;
DOI:10.1002/1099-0690(200205)2002:10<1654::AID-EJOC1654>3.0.CO;2-U

Reference yield:

: 95-51-2
o-chloroaniline

: 463342-71-4,148367-97-9
(1Z)-2-[(2-chlorophenyl)amino]-2-oxo-N-phenylethanehydrazonoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: 150 - 160 °C

2.1: SO₂Cl₂ / toluene

3.1: HCl; sodium nitrite / H₂O / 0 - 5 °C

3.2: 51 percent / sodium acetate / methanol; H₂O / 2 h / 5 - 10 °C

With hydrogenchloride; sulfuryl dichloride; sodium nitrite; In water; toluene; 3.2: Japp-Klingemann reaction;
DOI:10.1002/1099-0690(200205)2002:10<1654::AID-EJOC1654>3.0.CO;2-U

Reference yield:

: 93-70-9
3-oxo-N-2-chlorophenylbutanamide

: 463342-71-4,148367-97-9
(1Z)-2-[(2-chlorophenyl)amino]-2-oxo-N-phenylethanehydrazonoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: SO₂Cl₂ / toluene

2.1: HCl; sodium nitrite / H₂O / 0 - 5 °C

2.2: 51 percent / sodium acetate / methanol; H₂O / 2 h / 5 - 10 °C

With hydrogenchloride; sulfuryl dichloride; sodium nitrite; In water; toluene; 2.2: Japp-Klingemann reaction;
DOI:10.1002/1099-0690(200205)2002:10<1654::AID-EJOC1654>3.0.CO;2-U