2H-Benzimidazole-2-thione,1,3-dihydro-1,5-dimethyl-(9CI)

Base Information

• Chemical Name: 2H-Benzimidazole-2-thione,1,3-dihydro-1,5-dimethyl-(9CI)
• CAS No.: 149530-79-0
• Molecular Formula: C₉H₁₀N₂S
• Molecular Weight: 178.258
• Hs Code.: 2933990090
• Mol file: 149530-79-0.mol

Synonyms:2H-Benzimidazole-2-thione,1,3-dihydro-1,5-dimethyl-(9CI)

Chemical Property of 2H-Benzimidazole-2-thione,1,3-dihydro-1,5-dimethyl-(9CI)

Chemical Property:

• PSA: 56.62000
• LogP: 2.17040

Purity/Quality:

≥99% ^*data from raw suppliers

1,5-Dimethyl-1H-benzo[d]imidazole-2(3H)-thione 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2H-Benzimidazole-2-thione,1,3-dihydro-1,5-dimethyl-(9CI)

There total 2 articles about 2H-Benzimidazole-2-thione,1,3-dihydro-1,5-dimethyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,N-dimethyl-2-nitroaniline (4600-08-2) → 5-methylbenzimidazoline-2-thione (149530-79-0)

Guidance literature:

Multi-step reaction with 2 steps

1: tin; hydrochloric acid

With hydrogenchloride; tin;

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + 2-amino-4-methyl-N-methylaminobenzene (39513-19-4) → 5-methylbenzimidazoline-2-thione (149530-79-0)

Guidance literature:

Reference yield:

1-(bromoacetyl)-N-[2-(1H-pyrrol-1-yl)phenyl]-L-prolinamide (916143-43-6) + C9H10N2S (149530-79-0) → C26H27N5O2S (1018854-89-1)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 60 ℃; microwave irradiation;

DOI:10.1016/j.bmcl.2008.01.001

upstream raw materials:

carbon disulfide

2-amino-4-methyl-N-methylaminobenzene

4,N-dimethyl-2-nitroaniline

Downstream raw materials:

C₂₆H₂₇N₅O₂S

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