1H-Benzimidazole,2-(2-methylcyclopropyl)-(9CI)

Base Information

Chemical Name:1H-Benzimidazole,2-(2-methylcyclopropyl)-(9CI)
CAS No.:150649-20-0
Molecular Formula:C₁₁H₁₂N₂
Molecular Weight:172.23
Hs Code.:
Mol file:150649-20-0.mol

Synonyms:2-(2-Methylcyclopropyl)-1H-benzimidazole;2-(2-Methylcyclopropyl)-benzimidazole

Suppliers and Price of 1H-Benzimidazole,2-(2-methylcyclopropyl)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-(2-METHYLCYCLOPROPYL)-1H-BENZIMIDAZOLE 95.00%
5MG
$ 502.89

Total 1 raw suppliers

Chemical Property of 1H-Benzimidazole,2-(2-methylcyclopropyl)-(9CI)

Chemical Property:

Boiling Point:381.5±11.0 °C(Predicted)
PKA:11.95±0.10(Predicted)
PSA：0.00000
Density:1.203±0.06 g/cm3(Predicted)
LogP:0.00000

Purity/Quality:: 2-(2-METHYLCYCLOPROPYL)-1H-BENZIMIDAZOLE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1H-Benzimidazole,2-(2-methylcyclopropyl)-(9CI)

There total 3 articles about 1H-Benzimidazole,2-(2-methylcyclopropyl)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: N-(2-aminophenyl)-2-methylcyclopropanecarboxamide

: 150649-20-0
2-(2-methylcyclopropyl)-1H-benzimidazole

Guidance literature:: In acetic acid; for 3h; Reflux;
DOI:10.1016/j.tet.2013.02.021

Reference yield:

: 42274-66-8,52194-64-6,52194-65-7,60733-34-8
trans-2-methylcyclopropanecarboxylic acid chloride

: 150649-20-0
2-(2-methylcyclopropyl)-1H-benzimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / acetonitrile / 2 h / -25 - 20 °C

2: acetic acid / 3 h / Reflux

With triethylamine; In acetic acid; acetonitrile;
DOI:10.1016/j.tet.2013.02.021

Reference yield:

: 6142-57-0,6202-94-4,10487-86-2,14590-52-4,26510-98-5,29555-02-0,29667-48-9,122566-30-7
(+/-)-trans-2-methylcyclopropanecarboxylic acid

: 150649-20-0
2-(2-methylcyclopropyl)-1H-benzimidazole

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride; pyridine / diethyl ether / 1 h

2: triethylamine / acetonitrile / 2 h / -25 - 20 °C

3: acetic acid / 3 h / Reflux

With pyridine; thionyl chloride; triethylamine; In diethyl ether; acetic acid; acetonitrile;
DOI:10.1016/j.tet.2013.02.021