4-oxo-2-pyrimidinyl)-N,N-dimethyl-

Base Information

Chemical Name:4-oxo-2-pyrimidinyl)-N,N-dimethyl-
CAS No.:151587-54-1
Molecular Formula:C8H11 N5 O3
Molecular Weight:225.207
Hs Code.:
Mol file:151587-54-1.mol

Synonyms:Methanimidamide,N'-(1,4-dihydro-6-methyl-5-nitro-4-oxo-2-pyrimidinyl)-N,N-dimethyl- (9CI)

Suppliers and Price of 4-oxo-2-pyrimidinyl)-N,N-dimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-[(Dimethylamino)methylene]amino-6-methyl-5-nitro-4-pyrimidinol
50mg
$ 95.00

Biosynth Carbosynth
2-[(Dimethylamino)methylene]amino-6-methyl-5-nitro-4-pyrimidinol
500 mg
$ 840.00

Biosynth Carbosynth
2-[(Dimethylamino)methylene]amino-6-methyl-5-nitro-4-pyrimidinol
250 mg
$ 462.50

Biosynth Carbosynth
2-[(Dimethylamino)methylene]amino-6-methyl-5-nitro-4-pyrimidinol
100 mg
$ 255.00

Biosynth Carbosynth
2-[(Dimethylamino)methylene]amino-6-methyl-5-nitro-4-pyrimidinol
50 mg
$ 140.00

Total 3 raw suppliers

Chemical Property of 4-oxo-2-pyrimidinyl)-N,N-dimethyl-

Chemical Property:

Boiling Point:327.5±45.0 °C(Predicted)
PKA:6.69±0.50(Predicted)
PSA：107.43000
Density:1.42±0.1 g/cm3(Predicted)
LogP:1.14340
Solubility.:Chloroform, Dichloromethane

Purity/Quality:

97% ^*data from raw suppliers

2-[(Dimethylamino)methylene]amino-6-methyl-5-nitro-4-pyrimidinol ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses Intermediate in the preparation of 9-Deazaguanosine derivatives.

Technology Process of 4-oxo-2-pyrimidinyl)-N,N-dimethyl-

There total 2 articles about 4-oxo-2-pyrimidinyl)-N,N-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 4214-85-1
2-amino-6-methyl-5-nitro-4(3H)-oxopyrimidine

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 151587-54-1
2-<<(N,N-Dimethylamino)methylene>amino>-6-methyl-5-nitro-4(3H)-oxopyrimidine

Guidance literature:: In dichloromethane; at 20 ℃; for 1h;
DOI:10.1080/15257779908043082

Reference yield:

: 3977-29-5
2-amino-6-methyl-3H-pyrimidin-4-one

: 151587-54-1
2-<<(N,N-Dimethylamino)methylene>amino>-6-methyl-5-nitro-4(3H)-oxopyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / nitric acid / H₂SO₄ / 1 h / 50 °C

2: 92 percent / CH₂Cl₂ / 1 h / 20 °C

With nitric acid; In dichloromethane; sulfuric acid; 1: Nitration / 2: Condensation;
DOI:10.1080/15257779908043082