1,4-Bis(hexyloxy)-2,5-diiodobenzene

Base Information

Chemical Name:1,4-Bis(hexyloxy)-2,5-diiodobenzene
CAS No.:153033-31-9
Molecular Formula:C18H28 I2 O2
Molecular Weight:530.228
Hs Code.:
DSSTox Substance ID:DTXSID80514574
Nikkaji Number:J863.080A
Wikidata:Q82374973
Mol file:153033-31-9.mol

Synonyms:153033-31-9;1,4-BIS(HEXYLOXY)-2,5-DIIODOBENZENE;1,4-dihexoxy-2,5-diiodobenzene;1,4-DIIODO-2,5-BIS(HEXYLOXY)BENZENE;SCHEMBL1899569;DTXSID80514574

Suppliers and Price of 1,4-Bis(hexyloxy)-2,5-diiodobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1,4-Bis(hexyloxy)-2,5-diiodobenzene
1mg
$ 165.00

American Custom Chemicals Corporation
1,4-DIHEXYLOXY-2,5-DIIODOBENZENE 95.00%
5MG
$ 502.99

Total 1 raw suppliers

Chemical Property of 1,4-Bis(hexyloxy)-2,5-diiodobenzene

Chemical Property:

PSA：18.46000
LogP:6.81400
XLogP3:7.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:12
Exact Mass:530.01788
Heavy Atom Count:22
Complexity:238

Purity/Quality:: 1,4-Bis(hexyloxy)-2,5-diiodobenzene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCOC1=CC(=C(C=C1I)OCCCCCC)I
Uses 1,4-Bis(hexyloxy)-2,5-diiodobenzene is a reagent used in the post polymerization modification of polymers.

Technology Process of 1,4-Bis(hexyloxy)-2,5-diiodobenzene

There total 7 articles about 1,4-Bis(hexyloxy)-2,5-diiodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 67399-93-3
1,4-dihexyloxybenzene

: 153033-31-9
1,4-bis(hexyloxy)-2,5-diiodobenzene

Guidance literature:: With potassium iodate; sulfuric acid; iodine; acetic acid; In water; at 115 ℃; for 6h;
DOI:10.1002/ejoc.201001415

Reference yield: 27.0%

: 111-25-1
1-bromo-hexane

: 13064-64-7
2,5-diiodo-1,4-hydroquinone

: 357396-86-2
4-(hexyloxy)-2,5-diiodophenol

: 153033-31-9
1,4-bis(hexyloxy)-2,5-diiodobenzene

Guidance literature:: 1-bromo-hexane; 2,5-diiodo-1,4-hydroquinone; In ethanol; Heating;

With potassium hydroxide; In ethanol; for 3h; Further stages.; Heating;
DOI:10.1021/ja015614y

Reference yield:

: 111-25-1
1-bromo-hexane

: 153033-31-9
1,4-bis(hexyloxy)-2,5-diiodobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / K₂CO₃ / acetone / 3 h / Heating

2: 30 percent / KIO₃; I₂; acetic acid / H₂SO₄ / H₂O / 11 h / Heating

With potassium iodate; iodine; potassium carbonate; acetic acid; sulfuric acid; In water; acetone;
DOI:10.1016/j.tet.2004.03.059