Furan, 2-ethoxytetrahydro-3,4-dimethyl-5-pentyl-, (4R,5S)-rel- (9CI)

Base Information

Chemical Name:Furan, 2-ethoxytetrahydro-3,4-dimethyl-5-pentyl-, (4R,5S)-rel- (9CI)
CAS No.:671786-77-9
Molecular Formula:C13H26O2
Molecular Weight:214.34
Hs Code.:
Mol file:671786-77-9.mol

Synonyms:Furan, 2-ethoxytetrahydro-3,4-dimethyl-5-pentyl-, (4R,5S)-rel- (9CI)

Suppliers and Price of Furan, 2-ethoxytetrahydro-3,4-dimethyl-5-pentyl-, (4R,5S)-rel- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Furan, 2-ethoxytetrahydro-3,4-dimethyl-5-pentyl-, (4R,5S)-rel- (9CI)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of Furan, 2-ethoxytetrahydro-3,4-dimethyl-5-pentyl-, (4R,5S)-rel- (9CI)

There total 5 articles about Furan, 2-ethoxytetrahydro-3,4-dimethyl-5-pentyl-, (4R,5S)-rel- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 594-19-4
tert.-butyl lithium

: 2-ethoxy-4-iodomethyl-3-methyl-5-pentyltetrahydrofuran

: 671786-77-9
(4S,5R)-2-Ethoxy-3,4-dimethyl-5-pentyl-tetrahydro-furan

: 2,2-dimethyl-4-(2-pentyl-cyclopropyl)-pentan-3-ol

Guidance literature:: In diethyl ether;
DOI:10.1016/j.tet.2003.11.038

Reference yield:

: 3391-86-4
1-octen-3-ol

: 671786-77-9
(4S,5R)-2-Ethoxy-3,4-dimethyl-5-pentyl-tetrahydro-furan

Guidance literature:: Multi-step reaction with 3 steps

1: N-iodosuccinimide / CH₂Cl₂ / 2 h / 0 °C

2: 91 percent / triethylborane / hexane / 2 h / 20 °C

3: 38 percent / diethyl ether

With N-iodo-succinimide; triethyl borane; In diethyl ether; hexane; dichloromethane;
DOI:10.1016/j.tet.2003.11.038

Reference yield:

: 928-55-2
ethyl 1-propenyl ether

: 671786-77-9
(4S,5R)-2-Ethoxy-3,4-dimethyl-5-pentyl-tetrahydro-furan

Guidance literature:: Multi-step reaction with 3 steps

1: N-iodosuccinimide / CH₂Cl₂ / 2 h / 0 °C

2: 91 percent / triethylborane / hexane / 2 h / 20 °C

3: 38 percent / diethyl ether

With N-iodo-succinimide; triethyl borane; In diethyl ether; hexane; dichloromethane;
DOI:10.1016/j.tet.2003.11.038