D-gulo-Heptonic acid, 2,3,7-trideoxy-3,7-epithio-2,2-dimethyl-, gamma-lactone (9CI)

Base Information

Chemical Name:D-gulo-Heptonic acid, 2,3,7-trideoxy-3,7-epithio-2,2-dimethyl-, gamma-lactone (9CI)
CAS No.:601495-42-5
Molecular Formula:C₉H₁₄O₄S
Molecular Weight:218.274
Hs Code.:
Mol file:601495-42-5.mol

Synonyms:D-gulo-Heptonic acid, 2,3,7-trideoxy-3,7-epithio-2,2-dimethyl-, gamma-lactone (9CI)

Suppliers and Price of D-gulo-Heptonic acid, 2,3,7-trideoxy-3,7-epithio-2,2-dimethyl-, gamma-lactone (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of D-gulo-Heptonic acid, 2,3,7-trideoxy-3,7-epithio-2,2-dimethyl-, gamma-lactone (9CI)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of D-gulo-Heptonic acid, 2,3,7-trideoxy-3,7-epithio-2,2-dimethyl-, gamma-lactone (9CI)

There total 2 articles about D-gulo-Heptonic acid, 2,3,7-trideoxy-3,7-epithio-2,2-dimethyl-, gamma-lactone (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2-methyl-2-(2,3,4-tri-O-acetyl-5-thio-β-D-xylopyranosyl)propanoic acid methyl ester

: 601495-42-5
3,7-anhydro-2,2-dimethyl-4-thio-L-gluco-heptonic acid, γ-lactone

Guidance literature:: With sodium methylate; In methanol; for 1h;
DOI:10.1016/S0008-6215(03)00147-2

Reference yield:

: 130855-73-1
2,3,4-tri-O-acetyl-5-thio-β-D-xylopyranosyl bromide

: 601495-42-5
3,7-anhydro-2,2-dimethyl-4-thio-L-gluco-heptonic acid, γ-lactone

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / ZnCl₂ / CH₂Cl₂ / 1 h

2: 100 percent / NaOMe / methanol / 1 h

With sodium methylate; zinc(II) chloride; In methanol; dichloromethane;
DOI:10.1016/S0008-6215(03)00147-2