Cyclohexanecarboxaldehyde, 2-hydroxy-3,3-dimethyl-, (1S,2R)- (9CI)

Base Information

Chemical Name:Cyclohexanecarboxaldehyde, 2-hydroxy-3,3-dimethyl-, (1S,2R)- (9CI)
CAS No.:600726-40-7
Molecular Formula:C9H16O2
Molecular Weight:156.22214
Hs Code.:
Mol file:600726-40-7.mol

Synonyms:Cyclohexanecarboxaldehyde, 2-hydroxy-3,3-dimethyl-, (1S,2R)- (9CI)

Suppliers and Price of Cyclohexanecarboxaldehyde, 2-hydroxy-3,3-dimethyl-, (1S,2R)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Cyclohexanecarboxaldehyde, 2-hydroxy-3,3-dimethyl-, (1S,2R)- (9CI)

Chemical Property:

Boiling Point:235.3±33.0 °C(Predicted)
PKA:14.77±0.60(Predicted)
PSA：37.30000
Density:1.052±0.06 g/cm3(Predicted)
LogP:1.37250

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Cyclohexanecarboxaldehyde, 2-hydroxy-3,3-dimethyl-, (1S,2R)- (9CI)

There total 5 articles about Cyclohexanecarboxaldehyde, 2-hydroxy-3,3-dimethyl-, (1S,2R)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 600726-36-1
2,2-dimethyl-heptanedial

: 600726-40-7
2-hydroxy-3,3-dimethyl-cyclohexanecarbaldehyde

Guidance literature:: With L-proline; In dichloromethane; at 20 ℃;
DOI:10.1002/anie.200351266

Reference yield:

: 1193-47-1
2,2-dimethyl-cyclohexanone

: 600726-40-7
2-hydroxy-3,3-dimethyl-cyclohexanecarbaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride

2: diisobutylaluminium hydride

3: (S)-proline / CH₂Cl₂ / 20 °C

With sodium hydride; diisobutylaluminium hydride; L-proline; In dichloromethane; 2: retro-Dieckman condensation;
DOI:10.1002/anie.200351266

Reference yield:

: 101327-97-3
Methyl 3,3-dimethyl-2-oxocyclohexanecarboxylate

: 600726-40-7
2-hydroxy-3,3-dimethyl-cyclohexanecarbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride

2: (S)-proline / CH₂Cl₂ / 20 °C

With diisobutylaluminium hydride; L-proline; In dichloromethane; 1: retro-Dieckman condensation;
DOI:10.1002/anie.200351266