4-tert-Butyl 2-methyl 3-(2-methoxy-2-oxoethyl)-5-methyl-1H-pyrrole-2,4 -dicarboxylate

Base Information

Chemical Name:4-tert-Butyl 2-methyl 3-(2-methoxy-2-oxoethyl)-5-methyl-1H-pyrrole-2,4 -dicarboxylate
CAS No.:60024-79-5
Molecular Formula:C15H21NO6
Molecular Weight:0
Hs Code.:
Mol file:60024-79-5.mol

Synonyms:4-tert-Butyl 2-methyl 3-(2-methoxy-2-oxoethyl)-5-methyl-1H-pyrrole-2,4 -dicarboxylate;1H-Pyrrole-2,4-dicarboxylicacid,3-(2-methoxy-2-oxoethyl)-5-methyl-,4-(1,1-dimethylethyl)2-methylester(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-tert-Butyl 2-methyl 3-(2-methoxy-2-oxoethyl)-5-methyl-1H-pyrrole-2,4 -dicarboxylate

Chemical Property:

PSA：94.69000
LogP:1.78050

Purity/Quality:

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Technology Process of 4-tert-Butyl 2-methyl 3-(2-methoxy-2-oxoethyl)-5-methyl-1H-pyrrole-2,4 -dicarboxylate

There total 3 articles about 4-tert-Butyl 2-methyl 3-(2-methoxy-2-oxoethyl)-5-methyl-1H-pyrrole-2,4 -dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1694-31-1
tert-butyl acetoacetate

: 868-09-7
2-hydroxyimino-3-oxo-pentanedioic acid dimethyl ester

: 60024-79-5
methyl 3-<(methoxycarbonyl)methyl>-4-(tert-butoxycarbonyl)-5-methylpyrrole-2-carboxylate

Guidance literature:: With ammonium acetate; acetic acid; zinc; at 60 ℃; for 4h; Yield given;
DOI:10.1021/jo00374a031

Reference yield:

: 1830-54-2
3-oxopentanedioic acid dimethyl ester

: 60024-79-5
methyl 3-<(methoxycarbonyl)methyl>-4-(tert-butoxycarbonyl)-5-methylpyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: conc. HCl, amyl nitrite

2: glacial acetic acid, zinc, ammonium acetate / 4 h / 60 °C

With ammonium acetate; hydrogenchloride; n-Amyl nitrite; acetic acid; zinc;
DOI:10.1021/jo00374a031