ALPHA,ALPHA'-DIANILINO-P-XYLENE

Base Information

Chemical Name:ALPHA,ALPHA'-DIANILINO-P-XYLENE
CAS No.:13170-62-2
Molecular Formula:C20H20N2
Molecular Weight:288.392
Hs Code.:2921590090
Mol file:13170-62-2.mol

Synonyms:ALPHA,ALPHA'-DIANILINO-P-XYLENE;alph,alph-Dianilino-p-xylene;Dianilinoxylene

Suppliers and Price of ALPHA,ALPHA'-DIANILINO-P-XYLENE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
α,α''-dianilino-P-xylene
100mg
$ 65.00

TCI Chemical
α,α'-Dianilino-p-xylene >98.0%(GC)
1g
$ 124.00

TCI Chemical
α,α'-Dianilino-p-xylene >98.0%(GC)
5g
$ 422.00

Crysdot
N,N'-(1,4-Phenylenebis(methylene))dianiline 97%
5g
$ 340.00

Biosynth Carbosynth
a,a'-Dianilino-p-xylene
5 g
$ 306.00

Biosynth Carbosynth
a,a'-Dianilino-p-xylene
2 g
$ 153.00

Biosynth Carbosynth
a,a'-Dianilino-p-xylene
1 g
$ 88.00

Biosynth Carbosynth
a,a'-Dianilino-p-xylene
500 mg
$ 50.00

Biosynth Carbosynth
a,a'-Dianilino-p-xylene
10 g
$ 520.00

American Custom Chemicals Corporation
ALPHA,ALPHA'-DIANILINO-PARA-XYLENE 95.00%
5G
$ 1090.08

Total 10 raw suppliers

Chemical Property of ALPHA,ALPHA'-DIANILINO-P-XYLENE

Chemical Property:

Melting Point:127°C
Boiling Point:468.0±25.0 °C(Predicted)
PKA:4.09±0.10(Predicted)
Flash Point:295.2oC
PSA：24.06000
Density:1.154±0.06 g/cm3(Predicted)
LogP:5.05680

Purity/Quality:

99%, ^*data from raw suppliers

α,α''-dianilino-P-xylene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Statements: 36/37/38
Safety Statements: 26-36

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of ALPHA,ALPHA'-DIANILINO-P-XYLENE

There total 11 articles about ALPHA,ALPHA'-DIANILINO-P-XYLENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 623-27-8
terephthalaldehyde,

: 98-95-3,26969-40-4
nitrobenzene

: 13170-62-2
N,N'-(1,4-phenylene-bis(methylene))dianiline

Guidance literature:: With hydrogen; In methanol; at 20 ℃; for 8h; under 760.051 Torr;
DOI:10.1021/jo901787t

Reference yield: 82.0%

: 623-27-8
terephthalaldehyde,

: 62-53-3
aniline

: 13170-62-2
N,N'-(1,4-phenylene-bis(methylene))dianiline

Guidance literature:: With cobalt(II) phthalocyanine; diphenylsilane; In ethanol; at 70 ℃; for 12h; chemoselective reaction;
DOI:10.1002/adsc.201100645

Reference yield: 81.0%

: 29540-84-9
4-chlorophenyl trifluoromethanesulfonate

: 103-01-5
N-Phenylglycine

: 4750-61-2
N-(p-chlorobenzyl)aniline

: 13170-62-2
N,N'-(1,4-phenylene-bis(methylene))dianiline

Guidance literature:: With nickel(II) triflate; P(p-CH₃OC₆H₄)3; Ir(dFCF₃(ppy))2(4,4’-ditert-butyl-2,2’-bipyrididyl)PF₆; caesium carbonate; In acetonitrile; at 20 ℃; for 24h; Sealed tube; Irradiation; Inert atmosphere;
DOI:10.1002/chem.201604452