3-Furanaceticacid,2-ethyl-alpha-formyltetrahydro-5-oxo-,methylester,(2R,3R)-(9CI)

Base Information

Chemical Name:3-Furanaceticacid,2-ethyl-alpha-formyltetrahydro-5-oxo-,methylester,(2R,3R)-(9CI)
CAS No.:595583-80-5
Molecular Formula:C₁₀H₁₄O₅
Molecular Weight:214.218
Hs Code.:
Mol file:595583-80-5.mol

Synonyms:3-Furanaceticacid,2-ethyl-alpha-formyltetrahydro-5-oxo-,methylester,(2R,3R)-(9CI)

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Chemical Property of 3-Furanaceticacid,2-ethyl-alpha-formyltetrahydro-5-oxo-,methylester,(2R,3R)-(9CI)

Chemical Property:

PSA：69.67000
LogP:0.31620

Purity/Quality:

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Technology Process of 3-Furanaceticacid,2-ethyl-alpha-formyltetrahydro-5-oxo-,methylester,(2R,3R)-(9CI)

There total 3 articles about 3-Furanaceticacid,2-ethyl-alpha-formyltetrahydro-5-oxo-,methylester,(2R,3R)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 595583-79-2
((2R,3R)-2-Ethyl-5-oxo-tetrahydro-furan-3-yl)-ethylsulfanylcarbonyl-acetic acid methyl ester

: 595583-80-5
2-((2R,3R)-2-Ethyl-5-oxo-tetrahydro-furan-3-yl)-3-oxo-propionic acid methyl ester

Guidance literature:: With triethylsilane; palladium on activated charcoal; In acetone; at 20 ℃; for 3h;
DOI:10.1021/ol035128a

Reference yield:

: 76291-90-2
(-)-(R)-5-ethyl-2(5H)-furanone

: 595583-80-5
2-((2R,3R)-2-Ethyl-5-oxo-tetrahydro-furan-3-yl)-3-oxo-propionic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: t-BuOK / 2-methyl-propan-2-ol / 0.17 h / 20 °C

1.2: 88 percent / 2-methyl-propan-2-ol / 3 h / 20 °C

2.1: 100 percent / Et₃SiH / Pd/C / acetone / 3 h / 20 °C

With triethylsilane; potassium tert-butylate; palladium on activated charcoal; In acetone; tert-butyl alcohol;
DOI:10.1021/ol035128a

Reference yield:

: 595583-78-1
(Z)-(R)-4-(Tetrahydro-pyran-2-yloxy)-hex-2-enoic acid methyl ester

: 595583-80-5
2-((2R,3R)-2-Ethyl-5-oxo-tetrahydro-furan-3-yl)-3-oxo-propionic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: p-TsOH*H₂O / methanol / 1.5 h / 20 °C

2.1: t-BuOK / 2-methyl-propan-2-ol / 0.17 h / 20 °C

2.2: 88 percent / 2-methyl-propan-2-ol / 3 h / 20 °C

3.1: 100 percent / Et₃SiH / Pd/C / acetone / 3 h / 20 °C

With triethylsilane; potassium tert-butylate; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; acetone; tert-butyl alcohol;
DOI:10.1021/ol035128a