Technology Process of 5-Butan-2-yl-2-sulfanylidene-1,3-diazinane-4,6-dione
There total 1 articles about 5-Butan-2-yl-2-sulfanylidene-1,3-diazinane-4,6-dione which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium ethanolate;
In
ethanol;
at 20 ℃;
for 6h;
Heating / reflux;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium ethanolate / ethanol / 14 h / 20 °C
1.2: pH 2
2.1: N,N-dimethyl-aniline; trichlorophosphate / 2 h / 100 °C
With
sodium ethanolate; N,N-dimethyl-aniline; trichlorophosphate;
In
ethanol;
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: sodium ethanolate / ethanol / 14 h / 20 °C
1.2: pH 2
2.1: N,N-dimethyl-aniline; trichlorophosphate / 2 h / 100 °C
3.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C
3.2: 20 °C
4.1: trifluoroacetic acid / dichloromethane / 20 °C
5.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 2 h / 0 - 20 °C
6.1: potassium carbonate / N,N-dimethyl-formamide / 8 h / 20 - 60 °C
7.1: tetrahydrofuran / 72 h / 20 °C
8.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 0 - 20 °C
9.1: sodium hydrogencarbonate / 12 h / 150 °C
With
sodium ethanolate; sodium hydride; sodium hydrogencarbonate; potassium carbonate; N,N-dimethyl-aniline; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; trichlorophosphate;
In
tetrahydrofuran; ethanol; dichloromethane; chloroform; N,N-dimethyl-formamide;