Furan, 2-ethoxytetrahydro-4-methyl-3-(1-methylethyl)-, (2R,3R,4R)-rel- (9CI)

Base Information

Chemical Name:Furan, 2-ethoxytetrahydro-4-methyl-3-(1-methylethyl)-, (2R,3R,4R)-rel- (9CI)
CAS No.:586953-26-6
Molecular Formula:C10H20O2
Molecular Weight:172.26
Hs Code.:
Mol file:586953-26-6.mol

Synonyms:Furan, 2-ethoxytetrahydro-4-methyl-3-(1-methylethyl)-, (2R,3R,4R)-rel- (9CI)

Suppliers and Price of Furan, 2-ethoxytetrahydro-4-methyl-3-(1-methylethyl)-, (2R,3R,4R)-rel- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Furan, 2-ethoxytetrahydro-4-methyl-3-(1-methylethyl)-, (2R,3R,4R)-rel- (9CI)

Chemical Property:

Boiling Point:196.1±8.0 °C(Predicted)
PSA：18.46000
Density:0.90±0.1 g/cm3(Predicted)
LogP:2.28750

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Furan, 2-ethoxytetrahydro-4-methyl-3-(1-methylethyl)-, (2R,3R,4R)-rel- (9CI)

There total 4 articles about Furan, 2-ethoxytetrahydro-4-methyl-3-(1-methylethyl)-, (2R,3R,4R)-rel- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-bromo-1-ethoxy-3-methyl-1-(2-propenoxy)-butane

: 586953-26-6,217969-55-6
(r-2,t-3,c-4)-2-ethoxy-4-methyl-3-isopropyltetrahydrofuran

: 586953-26-6,217969-55-6
(r-2,c-3,c-4)-2-ethoxy-4-methyl-3-isopropyltetrahydrofuran

Guidance literature:: With air; triethyl borane; tri-n-butyl-tin hydride; In hexane; toluene; at -78 ℃; for 3h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0040-4039(98)01971-6

Reference yield:

: 2-bromo-1-ethoxy-3-methyl-1-(2-propenoxy)-butane

: 586953-26-6,217969-55-6
(r-2,t-3,c-4)-2-ethoxy-4-methyl-3-isopropyltetrahydrofuran

: 586953-26-6,217969-55-6
(r-2,c-3,c-4)-2-ethoxy-4-methyl-3-isopropyltetrahydrofuran

Guidance literature:: With air; triethyl borane; tri-n-butyl-tin hydride; In hexane; toluene; at -78 ℃; for 3h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0040-4039(98)01971-6

Reference yield:

: 30989-66-3
(Z/E)-1-ethoxy-3-methyl-1-butene

: 586953-26-6,217969-55-6
(r-2,t-3,c-4)-2-ethoxy-4-methyl-3-isopropyltetrahydrofuran

Guidance literature:: Multi-step reaction with 2 steps

1: 24 percent / NBS / CH₂Cl₂ / -20 °C

2: Bu₃SnH; Et₃B; O₂ / toluene; hexane / 3 h / -78 °C

With N-Bromosuccinimide; triethyl borane; oxygen; tri-n-butyl-tin hydride; In hexane; dichloromethane; toluene;
DOI:10.1002/chem.200390180