2,5,7-Metheno-1H-cyclopenta[a]pentalen-3-ol,decahydro-,(2S,3S,3aS,3bS,5S,6aR,7R,7aR,8R)-(9CI)

Base Information

Chemical Name:2,5,7-Metheno-1H-cyclopenta[a]pentalen-3-ol,decahydro-,(2S,3S,3aS,3bS,5S,6aR,7R,7aR,8R)-(9CI)
CAS No.:506441-55-0
Molecular Formula:C₁₂H₁₆O
Molecular Weight:176.258
Hs Code.:
Mol file:506441-55-0.mol

Synonyms:2,5,7-Metheno-1H-cyclopenta[a]pentalen-3-ol,decahydro-,(2S,3S,3aS,3bS,5S,6aR,7R,7aR,8R)-(9CI)

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Chemical Property of 2,5,7-Metheno-1H-cyclopenta[a]pentalen-3-ol,decahydro-,(2S,3S,3aS,3bS,5S,6aR,7R,7aR,8R)-(9CI)

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Technology Process of 2,5,7-Metheno-1H-cyclopenta[a]pentalen-3-ol,decahydro-,(2S,3S,3aS,3bS,5S,6aR,7R,7aR,8R)-(9CI)

There total 7 articles about 2,5,7-Metheno-1H-cyclopenta[a]pentalen-3-ol,decahydro-,(2S,3S,3aS,3bS,5S,6aR,7R,7aR,8R)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: (-)-pentacyclo[6.2.1.1^3,6.0^2,7.0^5,9]dodecan-4-one

: 506441-55-0,506441-57-2
(+)-endo-pentacyclo[6.2.1.1^3,6.0^2,7.0^5,9]dodecan-4-ol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 20 ℃; for 120h;
DOI:10.1016/S0957-4166(02)00549-9

Reference yield: 66.0%

: C₁₂H₈Cl₆O

: 7388-87-6,33163-93-8,33163-95-0,34378-86-4,38409-40-4,144787-48-4,144787-50-8,144787-53-1
(+/-)-endo-endo-tetracyclo[6.2.1.1^3,6.0^2,7]dodeca-9-en-4-exo-ol

: 506441-55-0,506441-57-2
(+/-)-exo-pentacyclo[6.2.1.1^3,6.0^2,7.0^5,9]dodecan-4-ol

Guidance literature:: C₁₂H₈Cl₆O; With ethanol; sodium; In tetrahydrofuran; ammonia; for 0.2h;

With silver nitrate; In diethyl ether; water; for 4h;
DOI:10.1016/S0957-4166(02)00549-9

Reference yield:

: 506441-55-0,506441-57-2
(+)-exo-pentacyclo[6.2.1.1^3,6.0^2,7.0^5,9]dodecan-4-ol

: 506441-55-0,506441-57-2
(+)-endo-pentacyclo[6.2.1.1^3,6.0^2,7.0^5,9]dodecan-4-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / pyridinium chlorochromate / CH₂Cl₂ / 4 h / 20 °C

2: 90 percent / LiAlH₄ / diethyl ether / 120 h / 20 °C

With lithium aluminium tetrahydride; pyridinium chlorochromate; In diethyl ether; dichloromethane;
DOI:10.1016/S0957-4166(02)00549-9