3-Iodo-7-methylimidazo[1,2-a]pyridine

Base Information

• Chemical Name: 3-Iodo-7-methylimidazo[1,2-a]pyridine
• CAS No.: 59938-33-9
• Molecular Formula: C8H7IN2
• Molecular Weight: 258.06
• European Community (EC) Number: 804-089-4
• DSSTox Substance ID: DTXSID90491842
• Wikidata: Q82336893
• Mol file: 59938-33-9.mol

Synonyms:3-Iodo-7-methylimidazo[1,2-a]pyridine;59938-33-9;3-IODO-7-METHYL-IMIDAZO[1,2-A]PYRIDINE;SCHEMBL10138747;DTXSID90491842;CC1=CC2=NC=C(I)N2C=C1;MFCD06739254;ZB1356;AKOS017560000;AB28973;FT-0752623;3-Iodo-7-methylimidazo[1,2-a]pyridine, 97%;E80297;EN300-2949261;A869085

Chemical Property of 3-Iodo-7-methylimidazo[1,2-a]pyridine

Chemical Property:

• Melting Point: 109-117°C
• PSA: 17.30000
• LogP: 2.24730
• Storage Temp.: ?20°C
• XLogP3: 2.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 257.96540
• Heavy Atom Count: 11
• Complexity: 151

Purity/Quality:

97% ^*data from raw suppliers

3-Iodo-7-methylimidazo[1,2-a]pyridine 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC2=NC=C(N2C=C1)I

Technology Process of 3-Iodo-7-methylimidazo[1,2-a]pyridine

There total 3 articles about 3-Iodo-7-methylimidazo[1,2-a]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7-Methyl-imidazo[1,2-a]pyridine (874-39-5) → 3-iodo-7-methylimidazo[1,2-a]pyridine (59938-33-9)

Guidance literature:

With N-iodo-succinimide; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

Reference yield:

2-Amino-4-methylpyridine (695-34-1) → 3-iodo-7-methylimidazo[1,2-a]pyridine (59938-33-9)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / Reflux

2: N-iodo-succinimide / acetonitrile

With N-iodo-succinimide; In ethanol; acetonitrile;

DOI:10.1021/acs.jmedchem.0c02064

Reference yield:

→ 3-iodo-7-methylimidazo[1,2-a]pyridine (59938-33-9)

Guidance literature:

Verb. 4, NaOH / Me., I2 / Me.;

DOI:10.1021/jo00884a013

upstream raw materials:

7-Methyl-imidazo[1,2-a]pyridine

2-Amino-4-methylpyridine

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