Benzoic acid, 4-[[(5-methyl-2-furanyl)carbonyl]amino]-, methyl ester (9CI)

Base Information

• Chemical Name: Benzoic acid, 4-[[(5-methyl-2-furanyl)carbonyl]amino]-, methyl ester (9CI)
• CAS No.: 540533-39-9
• Molecular Formula: C14H13NO4
• Molecular Weight: 259.262
• Mol file: 540533-39-9.mol

Synonyms:Benzoic acid, 4-[[(5-methyl-2-furanyl)carbonyl]amino]-, methyl ester (9CI)

Chemical Property of Benzoic acid, 4-[[(5-methyl-2-furanyl)carbonyl]amino]-, methyl ester (9CI)

Chemical Property:

• PSA: 72.03000
• LogP: 3.01090

Purity/Quality:

99% ^*data from raw suppliers

Methyl4-[(5-methylfuran-2-carbonyl)amino]benzoate 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 4-[[(5-methyl-2-furanyl)carbonyl]amino]-, methyl ester (9CI)

There total 1 articles about Benzoic acid, 4-[[(5-methyl-2-furanyl)carbonyl]amino]-, methyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.75%

5-methylfuran-2-carbonyl chloride (14003-11-3) + 4-methoxycarbonyl aniline (619-45-4) → methyl 4-(5-methylfuran-2-carboxamido)benzoate (540533-39-9)

Guidance literature:

With potassium carbonate; In dichloromethane; at 20 ℃;

Reference yield: 57.0%

1-[4-(4-methoxyphenyl)tetrahydro-2H-pyran-4-yl]-methylamine (440087-51-4) + methyl 4-(5-methylfuran-2-carboxamido)benzoate (540533-39-9) → N-(4-((tetrahydro-4-(4-methoxyphenyl)-2H-pyran-4-yl)methylcarbamoyl)phenyl)-5-methylfuran-2-carboxamide (1445796-95-1)

Guidance literature:

With trimethylaluminum; In toluene; Reflux;

upstream raw materials:

5-methylfuran-2-carbonyl chloride

4-methoxycarbonyl aniline

Downstream raw materials:

N-(4-((tetrahydro-4-(4-methoxyphenyl)-2H-pyran-4-yl)methylcarbamoyl)phenyl)-5-methylfuran-2-carboxamide

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