Cyclopropanecarboxaldehyde, 2,2,3-trimethyl-3-nitro-, (1R,3S)- (9CI)

Base Information

Chemical Name:Cyclopropanecarboxaldehyde, 2,2,3-trimethyl-3-nitro-, (1R,3S)- (9CI)
CAS No.:518352-35-7
Molecular Formula:C7H11NO3
Molecular Weight:157.16714
Hs Code.:
Mol file:518352-35-7.mol

Synonyms:Cyclopropanecarboxaldehyde, 2,2,3-trimethyl-3-nitro-, (1R,3S)- (9CI)

Suppliers and Price of Cyclopropanecarboxaldehyde, 2,2,3-trimethyl-3-nitro-, (1R,3S)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclopropanecarboxaldehyde, 2,2,3-trimethyl-3-nitro-, (1R,3S)- (9CI)

Chemical Property:

PSA：62.89000
LogP:1.39990

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Cyclopropanecarboxaldehyde, 2,2,3-trimethyl-3-nitro-, (1R,3S)- (9CI)

There total 2 articles about Cyclopropanecarboxaldehyde, 2,2,3-trimethyl-3-nitro-, (1R,3S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 518352-34-6
(S)-1-((1R,3S)-2,2,3-Trimethyl-3-nitro-cyclopropyl)-ethane-1,2-diol

: 518352-35-7
(1R,2R)-trans-2,3,3-trimethyl-2-nitro-cyclopropancarbaldehyde

Guidance literature:: With sodium periodate; phosphate buffer; In methanol; water; at 20 ℃; for 2h; pH=7;
DOI:10.1016/S0040-4020(02)01406-0

Reference yield:

: 182682-35-5
(4S,1R,3R)-trans-2,2-dimethyl-4-(2,3,3-trimethyl-2-nitro-cyclopropyl)-[1,3]dioxolane

: 518352-35-7
(1R,2R)-trans-2,3,3-trimethyl-2-nitro-cyclopropancarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / p-TsOH / methanol; H₂O / 18 h / 20 °C

2: 77 percent / NaIO₄; phosphate buffer / methanol; H₂O / 2 h / 20 °C / pH 7

With sodium periodate; phosphate buffer; toluene-4-sulfonic acid; In methanol; water;
DOI:10.1016/S0040-4020(02)01406-0