N,N-Diethyl-4-nitrosoaniline hydrochloride

Base Information

• Chemical Name: N,N-Diethyl-4-nitrosoaniline hydrochloride
• CAS No.: 53743-85-4
• Molecular Formula: C₁₀H₁₄N₂O*ClH
• Molecular Weight: 214.695
• Hs Code.: 2921420090
• European Community (EC) Number: 626-189-5
• DSSTox Substance ID: DTXSID50584300
• Mol file: 53743-85-4.mol

Synonyms:N,N-Diethyl-4-nitrosoaniline hydrochloride;53743-85-4;N,N-diethyl-4-nitrosoaniline;hydrochloride;N N-DIETHYL-4-NITROSOANILINE HYDROCHLOR&;SCHEMBL11586430;DTXSID50584300;N,N-di-ethyl-p-nitrosoaniline hydrochloride;N,N-Diethyl-4-nitrosoaniline--hydrogen chloride (1/1)

Chemical Property of N,N-Diethyl-4-nitrosoaniline hydrochloride

Chemical Property:

• Melting Point: 107 °C(lit.)
• PSA: 32.67000
• LogP: 3.73270
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 214.0872908
• Heavy Atom Count: 14
• Complexity: 149

Purity/Quality:

95%+ or 98%+ ^*data from raw suppliers

N,N-DIETHYL-4-NITROSOANILINE HYDROCHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN(CC)C1=CC=C(C=C1)N=O.Cl

Technology Process of N,N-Diethyl-4-nitrosoaniline hydrochloride

There total 1 articles about N,N-Diethyl-4-nitrosoaniline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ N,N-diethyl-4-nitroso-aniline; dihydrochloride (53743-85-4,58066-98-1)

Guidance literature:

With hydrogenchloride;

Reference yield:

N,N-diethyl-4-nitrosoaniline hydrochloride (53743-85-4) → C27H25N3O2 (1337469-24-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: zinc(II) chloride / ethanol / Reflux

2.1: ethanol / 72 h / Reflux

2.2: 3 h / 20 °C / pH 9

With zinc(II) chloride; In ethanol;

DOI:10.1016/j.bmcl.2011.07.112

Reference yield:

N,N-diethyl-4-nitrosoaniline hydrochloride (53743-85-4) → C27H25N3O2 (1337469-25-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: zinc(II) chloride / ethanol / Reflux

2.1: ethanol / 72 h / Reflux

2.2: 3 h / 20 °C / pH 9

With zinc(II) chloride; In ethanol;

DOI:10.1016/j.bmcl.2011.07.112

Downstream raw materials:

C₂₆H₂₃N₃O

C₂₇H₂₅N₃O

C₂₆H₂₁ClN₄O₃

C₂₇H₂₁N₅O₃