Bicyclo[2.2.1]hepta-2,5-diene-2-carboxaldehyde, 5,6-dimethyl- (9CI)

Base Information

Chemical Name:Bicyclo[2.2.1]hepta-2,5-diene-2-carboxaldehyde, 5,6-dimethyl- (9CI)
CAS No.:56775-40-7
Molecular Formula:C₁₀H₁₂O
Molecular Weight:148.205
Hs Code.:
Mol file:56775-40-7.mol

Synonyms:Bicyclo[2.2.1]hepta-2,5-diene-2-carboxaldehyde, 5,6-dimethyl- (9CI)

Suppliers and Price of Bicyclo[2.2.1]hepta-2,5-diene-2-carboxaldehyde, 5,6-dimethyl- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of Bicyclo[2.2.1]hepta-2,5-diene-2-carboxaldehyde, 5,6-dimethyl- (9CI)

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Bicyclo[2.2.1]hepta-2,5-diene-2-carboxaldehyde, 5,6-dimethyl- (9CI)

There total 3 articles about Bicyclo[2.2.1]hepta-2,5-diene-2-carboxaldehyde, 5,6-dimethyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 624-67-9
Propargylic aldehyde

: 60924-88-1
(±)-2,3-dimethyl-2-cyclopenten-1-ol

: 56775-40-7
2-Formyl-5,6-dimethylbicyclo<2.2.1>hepta-2,5-diene

Guidance literature:: With magnesium sulfate; toluene-4-sulfonic acid; In benzene; at 3 - 10 ℃; for 6.5h;
DOI:10.1021/jo01296a022

Reference yield:

: 1121-05-7
2,3-dimethylcyclopent-2-enone

: 56775-40-7
2-Formyl-5,6-dimethylbicyclo<2.2.1>hepta-2,5-diene

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / LiAlH₄

2: p-Toluenesulfonic acid, MgSO₄ / benzene / 6.5 h / 3 - 10 °C

With lithium aluminium tetrahydride; magnesium sulfate; toluene-4-sulfonic acid; In benzene;
DOI:10.1021/jo01296a022