HYDANTOIN-5-ACETYL CHLORIDE, 95

Base Information

• Chemical Name: HYDANTOIN-5-ACETYL CHLORIDE, 95
• CAS No.: 51876-11-0
• Molecular Formula: C5H5ClN2O3
• Molecular Weight: 176.56
• Hs Code.: 2933990090
• Mol file: 51876-11-0.mol

Synonyms:HYDANTOIN-5-ACETYL CHLORIDE, 95

Chemical Property of HYDANTOIN-5-ACETYL CHLORIDE, 95

Chemical Property:

• Refractive Index: 1.495
• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 82.25000
• Density: 1.473g/cm³
• LogP: -0.73420

Purity/Quality:

99%, ^*data from raw suppliers

Hydantoin-5-acetylChloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s): R34:Causes burns.
• Hazard Codes: R34:Causes burns.
• Statements: R34:Causes burns.
• Safety Statements: S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.; S36/37/39:Wear suitabl

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of HYDANTOIN-5-ACETYL CHLORIDE, 95

There total 2 articles about HYDANTOIN-5-ACETYL CHLORIDE, 95 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

5-hydantoinacetic acid (5427-26-9) → (2,5-dioxo-imidazolidin-4-yl)-acetyl chloride (51876-11-0)

Guidance literature:

With thionyl chloride; at 89 ℃; for 120h; Heating / reflux;

Reference yield:

→ (2,5-dioxo-imidazolidin-4-yl)-acetyl chloride (51876-11-0)

Guidance literature:

Aus Hydantoin-5-essigsaeure und SOCl2;

DOI:10.1016/S0031-9422(00)91227-5

Reference yield:

4-chloro-aniline (106-47-8) + (2,5-dioxo-imidazolidin-4-yl)-acetyl chloride (51876-11-0) → N-(4-chloro-phenyl)-2-(2,4-dioxo-imidazolidin-5-yl)-acetamide (1008011-50-4)

Guidance literature:

With triethylamine; In 1,4-dioxane; at 100 ℃; for 0.166667h;

DOI:10.1016/j.ejmech.2009.02.023

upstream raw materials:

5-hydantoinacetic acid

Downstream raw materials:

N-(4-chloro-phenyl)-2-(2,4-dioxo-imidazolidin-5-yl)-acetamide

2-(2,4-dioxo-imidazolidin-5-yl)-N-(4-sulfamoyl-phenyl)-acetamide

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