1(2H)-Naphthalenone, 3,4-dihydro-2-hydroxy-6-methoxy-4,7-dimethyl-, (2S,4R)- (9CI)

Base Information

Chemical Name:1(2H)-Naphthalenone, 3,4-dihydro-2-hydroxy-6-methoxy-4,7-dimethyl-, (2S,4R)- (9CI)
CAS No.:477199-83-0
Molecular Formula:C13H16O3
Molecular Weight:220.26434
Hs Code.:
Mol file:477199-83-0.mol

Synonyms:1(2H)-Naphthalenone, 3,4-dihydro-2-hydroxy-6-methoxy-4,7-dimethyl-, (2S,4R)- (9CI)

Suppliers and Price of 1(2H)-Naphthalenone, 3,4-dihydro-2-hydroxy-6-methoxy-4,7-dimethyl-, (2S,4R)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1(2H)-Naphthalenone, 3,4-dihydro-2-hydroxy-6-methoxy-4,7-dimethyl-, (2S,4R)- (9CI)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1(2H)-Naphthalenone, 3,4-dihydro-2-hydroxy-6-methoxy-4,7-dimethyl-, (2S,4R)- (9CI)

There total 38 articles about 1(2H)-Naphthalenone, 3,4-dihydro-2-hydroxy-6-methoxy-4,7-dimethyl-, (2S,4R)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: (+)-aristelegone B

: 220570-40-1,477199-83-0
(+)-(2R,4S)-2-hydroxy-6-methoxy-4,7-dimethyl-3,4-dihydronaphthalen-1(2H)-one

Guidance literature:: With potassium carbonate; In methanol; at 0 ℃; for 1h; stereoselective reaction; Inert atmosphere;
DOI:10.1039/c5ob01740h

Reference yield: 54.0%

: 108-05-4,9003-20-7
vinyl acetate

: 130921-11-8,130921-12-9,477199-83-0
(±)-2-hydroxy-6-methoxy-4,7-dimethyl-3,4-dihydronaphthalen-1(2H)-one

: (+)-aristelegone B

: 477199-83-0
(-)-aristelegone B

Guidance literature:: With Lipase Amano PS; In acetone; at 25 ℃; for 36h; Solvent; stereoselective reaction; Enzymatic reaction;
DOI:10.1039/c5ob01740h

Reference yield:

: 130921-10-7
(±)-methoxy-4,7-dimethyl-3,4-dihydronaphthalen-1(2H)-one

: 220570-40-1,477199-83-0
(+)-(2R,4S)-2-hydroxy-6-methoxy-4,7-dimethyl-3,4-dihydronaphthalen-1(2H)-one

: 477199-83-0
(-)-aristelegone B

Guidance literature:: With bis-[(trifluoroacetoxy)iodo]benzene; potassium hydroxide; at 0 - 20 ℃; for 3h; Overall yield = 68 percent; Overall yield = 27 mg; Inert atmosphere;