Carbamic acid, (1R,3R,4S)-1-azabicyclo[2.2.1]hept-3-yl-, 1,1-dimethylethyl

Base Information

Chemical Name:Carbamic acid, (1R,3R,4S)-1-azabicyclo[2.2.1]hept-3-yl-, 1,1-dimethylethyl
CAS No.:473795-32-3
Molecular Formula:C11H20N2O2
Molecular Weight:212.29
Hs Code.:
Mol file:473795-32-3.mol

Synonyms:(1R,3R,4S)-REL-3-(BOC-AMINO)-1-AZABICYCLO[2.2.1]HEPTANE;

Suppliers and Price of Carbamic acid, (1R,3R,4S)-1-azabicyclo[2.2.1]hept-3-yl-, 1,1-dimethylethyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Synthonix
(1R,3R,4S)-rel-3-(Boc-amino)-1-azabicyclo[2.2.1]heptane 95+%
1g
$ 930.00

Synthonix
(1R,3R,4S)-rel-3-(Boc-amino)-1-azabicyclo[2.2.1]heptane 95+%
10g
$ 5370.00

Synthonix
(1R,3R,4S)-rel-3-(Boc-amino)-1-azabicyclo[2.2.1]heptane 95+%
5g
$ 3170.00

Matrix Scientific
(1R,3R,4S)-Rel-3-(Boc-amino)-1-azabicyclo[2.2.1]heptane 95+%
1g
$ 1634.00

Crysdot
(1R,3R,4S)-Rel-3-(Boc-amino)-1-azabicyclo[2.2.1]heptane 95+%
1g
$ 991.00

ACHEMBLOCK
(1r,3r,4s)-rel-3-(boc-amino)-1-azabicyclo[2.2.1]heptane 97%
250MG
$ 520.00

Total 5 raw suppliers

Chemical Property of Carbamic acid, (1R,3R,4S)-1-azabicyclo[2.2.1]hept-3-yl-, 1,1-dimethylethyl

Chemical Property:

Boiling Point:308.9±21.0 °C(Predicted)
PKA:12.39±0.20(Predicted)
PSA：45.06000
Density:1.10±0.1 g/cm3(Predicted)
LogP:1.35750

Purity/Quality:

97% ^*data from raw suppliers

(1R,3R,4S)-rel-3-(Boc-amino)-1-azabicyclo[2.2.1]heptane 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, (1R,3R,4S)-1-azabicyclo[2.2.1]hept-3-yl-, 1,1-dimethylethyl

There total 16 articles about Carbamic acid, (1R,3R,4S)-1-azabicyclo[2.2.1]hept-3-yl-, 1,1-dimethylethyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: (1R,3R,4S)-1-Benzyl-3-tert-butoxycarbonylamino-1-azonia-bicyclo[2.2.1]heptane

: 688790-05-8,473795-32-3
(3R,4S)-3-(tert-butoxycarbonylamino)-1-azabicyclo[2.2.1]heptane

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 48h; under 2585.74 Torr;
DOI:10.1016/j.bmc.2006.09.019

Reference yield: 47.0%

: 473795-30-1
trans (tert-butoxycarbonylamino)-exo-4-R-(2-hydroxyethyl)-1-(N-phenylmethyl)-3-pyrrolidine

: 473795-32-3
exo 3-(tert-butoxycarbonylamino)-1-azabicyclo[2.2.1]heptane

Guidance literature:: trans (tert-butoxycarbonylamino)-exo-4-R-(2-hydroxyethyl)-1-(N-phenylmethyl)-3-pyrrolidine; With methanesulfonyl chloride; triethylamine; In dichloromethane; at 0 ℃; for 0.166667h;

With hydrogen; palladium 10% on activated carbon; In ethanol; under 2740.96 Torr; Heating / reflux;

Reference yield: 46.0%

: trans-3-(tert-butoxycarbonylamino)-4-(2-hydroxyethyl)-1-(N-phenylmethyl)pyrrolidine

: 688790-05-8,473795-32-3
exo 3-(tert-butoxycarbonylamino)-1-azabicyclo[2.2.1]heptane

Guidance literature:: trans-3-(tert-butoxycarbonylamino)-4-(2-hydroxyethyl)-1-(N-phenylmethyl)pyrrolidine; With methanesulfonyl chloride; triethylamine; In dichloromethane;

In ethanol; for 16h; Heating / reflux;

With hydrogen; palladium 10% on activated carbon; at 20 ℃; under 2740.96 Torr;