alpha-L-lyxo-Hexopyranoside, methyl 3,4-diamino-2,3,4,6-tetradeoxy- (9CI)

Base Information

Chemical Name:alpha-L-lyxo-Hexopyranoside, methyl 3,4-diamino-2,3,4,6-tetradeoxy- (9CI)
CAS No.:491613-79-7
Molecular Formula:C7H16N2O2
Molecular Weight:160.21
Hs Code.:
Mol file:491613-79-7.mol

Synonyms:alpha-L-lyxo-Hexopyranoside, methyl 3,4-diamino-2,3,4,6-tetradeoxy- (9CI)

Suppliers and Price of alpha-L-lyxo-Hexopyranoside, methyl 3,4-diamino-2,3,4,6-tetradeoxy- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of alpha-L-lyxo-Hexopyranoside, methyl 3,4-diamino-2,3,4,6-tetradeoxy- (9CI)

Chemical Property:

PSA：70.50000
LogP:0.82290

Purity/Quality:

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Technology Process of alpha-L-lyxo-Hexopyranoside, methyl 3,4-diamino-2,3,4,6-tetradeoxy- (9CI)

There total 5 articles about alpha-L-lyxo-Hexopyranoside, methyl 3,4-diamino-2,3,4,6-tetradeoxy- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 637005-31-3
methyl 3,4-diazido-2,3,4,6-tetradeoxy-α-L-lyxo-hexopyranoside

: 491613-79-7
O-methyl 3,4-diamino-2,3,4,6-tetradeoxy-α-L-lyxohexopyranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 2h; under 2585.81 Torr;
DOI:10.1039/b212681h

Reference yield:

: 128164-26-1
tert-butyldimethylsilyl 3-azido-2,3,6-trideoxy-4-O-trifluoromethanesulfonyl-β-L-arabino-hexopyranoside

: 491613-79-7
O-methyl 3,4-diamino-2,3,4,6-tetradeoxy-α-L-lyxohexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 225.9 mg / sodium azide / dimethylformamide / 20 °C

2: 92.4 percent / 4A MS / CH₂Cl₂ / 2 h / 20 °C

3: 87 percent / H₂ / Pd/C / ethanol / 2 h / 2585.81 Torr

With sodium azide; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b212681h

Reference yield:

: 128135-56-8
4-O-acetyl-3-azido-1-O-tert-butyl(dimethyl)silyl-2,3,6-trideoxy-β-L-arabino-hexopyranose

: 491613-79-7
O-methyl 3,4-diamino-2,3,4,6-tetradeoxy-α-L-lyxohexopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 91.5 percent / K₂CO₃ / methanol / 20 °C

2: pyridine / CH₂Cl₂

3: 225.9 mg / sodium azide / dimethylformamide / 20 °C

4: 92.4 percent / 4A MS / CH₂Cl₂ / 2 h / 20 °C

5: 87 percent / H₂ / Pd/C / ethanol / 2 h / 2585.81 Torr

With pyridine; sodium azide; hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b212681h