1-benzyl hydrogen (S)-pyrrolidine-1,2-dicarboxylate, compound with dicyclohexylamine (1:1)

Base Information

Chemical Name:1-benzyl hydrogen (S)-pyrrolidine-1,2-dicarboxylate, compound with dicyclohexylamine (1:1)
CAS No.:26607-48-7
Molecular Formula:C25H38N2O4
Molecular Weight:430.588
Hs Code.:

Synonyms:compound with dicyclohexyl-amine;(S)-Pyrrolidine-1,2-dicarboxylic acid 1-benzyl ester;

Suppliers and Price of 1-benzyl hydrogen (S)-pyrrolidine-1,2-dicarboxylate, compound with dicyclohexylamine (1:1)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1-benzyl hydrogen (S)-pyrrolidine-1,2-dicarboxylate, compound with dicyclohexylamine (1:1)

Chemical Property:

Vapor Pressure:3.12E-15mmHg at 25°C
Boiling Point:599.7°C at 760 mmHg
Flash Point:316.5°C
PSA：78.87000
LogP:5.44240

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-benzyl hydrogen (S)-pyrrolidine-1,2-dicarboxylate, compound with dicyclohexylamine (1:1)

There total 1 articles about 1-benzyl hydrogen (S)-pyrrolidine-1,2-dicarboxylate, compound with dicyclohexylamine (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 101-83-7
N-cyclohexyl-cyclohexanamine

: 147-85-3,25191-13-3,37159-97-0,4305-67-3,4607-28-7
L-proline

: 26607-48-7
1-benzyl hydrogen (S)-pyrrolidine-1,2-dicarboxylate, compound with dicyclohexylamine (1:1)

Guidance literature:: With sodium hydroxide; Multistep reaction; 1.) 5 deg C, 15 min 2.) ethyl acetate, Et₂O, 5 min;
DOI:10.1016/S0040-4020(01)87839-X

Reference yield:

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 26607-48-7
1-benzyl hydrogen (S)-pyrrolidine-1,2-dicarboxylate, compound with dicyclohexylamine (1:1)

: 61058-42-2
Z-Pro-Gly-OMe

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; for 2h; temperature: below 0 deg C;
DOI:10.1016/S0040-4020(01)87839-X

Reference yield:

: 623-33-6
glycine ethyl ester hydrochloride

: 26607-48-7
1-benzyl hydrogen (S)-pyrrolidine-1,2-dicarboxylate, compound with dicyclohexylamine (1:1)

: 2766-31-6
ethyl (N-benzoxycarbonyl-L-prolyl)glycinate

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; for 2h; temperature: below 0 deg C;
DOI:10.1016/S0040-4020(01)87839-X