(1,3-Benzodioxol-5-ylmethyl)hydrazine

Base Information

• Chemical Name: (1,3-Benzodioxol-5-ylmethyl)hydrazine
• CAS No.: 51421-35-3
• Molecular Formula: C8H10N2O2
• Molecular Weight: 166.18
• Hs Code.: 2934999090
• DSSTox Substance ID: DTXSID90329035
• Wikidata: Q82092018
• Mol file: 51421-35-3.mol

Synonyms:51421-35-3;(1,3-benzodioxol-5-ylmethyl)hydrazine;BENZO[1,3]DIOXOL-5-YLMETHYL-HYDRAZINE;1,3-benzodioxol-5-ylmethylhydrazine;(Benzo[d][1,3]dioxol-5-ylmethyl)hydrazine;NCIOpen2_004467;SCHEMBL8722263;3,4-methylenedioxybenzylhydrazine;DTXSID90329035;BCA42135;MFCD07773081;STL444366;AKOS000151743;[(1,3-dioxaindan-5-yl)methyl]hydrazine;BB 0220357;[(2H-1,3-Benzodioxol-5-yl)methyl]hydrazine;EN300-270874;Benzo[1,3]dioxol-5-ylmethyl-hydrazinehydrochloride

Chemical Property of (1,3-Benzodioxol-5-ylmethyl)hydrazine

Chemical Property:

• Vapor Pressure: 5.2E-05mmHg at 25°C
• Refractive Index: 1.603
• Boiling Point: 347.9°C at 760 mmHg
• Flash Point: 164.2°C
• PSA: 56.51000
• Density: 1.284g/cm³
• LogP: 1.46980
• XLogP3: 0.6
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 166.074227566
• Heavy Atom Count: 12
• Complexity: 154

Purity/Quality:

98%min ^*data from raw suppliers

Benzo[1,3]dioxol-5-ylmethyl-hydrazine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1OC2=C(O1)C=C(C=C2)CNN

Technology Process of (1,3-Benzodioxol-5-ylmethyl)hydrazine

There total 4 articles about (1,3-Benzodioxol-5-ylmethyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

{3,4-(OCH2O)2C6H3C(H)=N-}2 (3510-50-7,134691-72-8) → Piperonyl-hydrazin (51421-35-3)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium amalgam; alcohol

2: yellow mercury oxide; alcohol / 50 - 60 °C

3: hydrochloric acid / durch Destillieren mit Wasserdampf

With hydrogenchloride; sodium amalgam; ethanol; mercury(II) oxide;

Reference yield:

piperonal-piperonylhydrazone → Piperonyl-hydrazin (51421-35-3)

Guidance literature:

With hydrogenchloride; durch Destillieren mit Wasserdampf;

Reference yield:

N,N'-dipiperonyl-hydrazine (92967-27-6) → Piperonyl-hydrazin (51421-35-3)

Guidance literature:

Multi-step reaction with 2 steps

1: yellow mercury oxide; alcohol / 50 - 60 °C

2: hydrochloric acid / durch Destillieren mit Wasserdampf

With hydrogenchloride; ethanol; mercury(II) oxide;

upstream raw materials:

N,N'-dipiperonyl-hydrazine

{3,4-(OCH₂O)2C₆H₃C(H)=N-}2

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