9-[bromo(phenyl)methyl]-10-phenylanthracene

Base Information

• Chemical Name: 9-[bromo(phenyl)methyl]-10-phenylanthracene
• CAS No.: 7467-97-2
• Molecular Formula: C₂₇H₁₉Br
• Molecular Weight: 423.352
• Mol file: 7467-97-2.mol

Synonyms:Anthracene,9-(a-bromobenzyl)-10-phenyl- (8CI);NSC 400711

Chemical Property of 9-[bromo(phenyl)methyl]-10-phenylanthracene

Chemical Property:

• Vapor Pressure: 3.66E-11mmHg at 25°C
• Boiling Point: 539.5°C at 760 mmHg
• Flash Point: 259°C
• Density: 1.338g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 9-[bromo(phenyl)methyl]-10-phenylanthracene

There total 8 articles about 9-[bromo(phenyl)methyl]-10-phenylanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-benzyl-10-phenyl-anthracene (24451-64-7) → 9-(α-bromo-benzyl)-10-phenyl-anthracene (7467-97-2)

Guidance literature:

With carbon disulfide; bromine;

DOI:10.1080/00139150209605596

Reference yield:

9-benzylidene-10-phenyl-10-hydroxy-9,10-dihydroanthracene (18084-17-8) → 9-(α-bromo-benzyl)-10-phenyl-anthracene (7467-97-2)

Guidance literature:

With hydrogen bromide; acetic acid;

DOI:10.1080/00139150209605596

Reference yield:

benzylideneanthrone (14343-92-1) → 9-(α-bromo-benzyl)-10-phenyl-anthracene (7467-97-2)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: glacial acetic acid; HBr

With diethyl ether; hydrogen bromide; acetic acid;

DOI:10.1080/00139150209605596

upstream raw materials:

9-benzyl-10-phenyl-anthracene

9-benzylidene-10-phenyl-10-hydroxy-9,10-dihydroanthracene

(10-phenylanthracen-9-yl)benzyl alcohol

hydrogen bromide